GCMS analysis results for sample AE06958, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

’ Data File : C:\MSDCHEM\l\DATA\041702\6958.D Vial: 12 Acq On : 17 Apr 2002 5:46 pm Operator: Bohllc Sample : SAMPLE 6958 3/25/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.93 1.54 ug/L 183552 Naphthalene-d8 12.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 50 3 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 40 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H22O3Si2 003789-85-3 40 Abundance Scan 1506 (11.928 min): 6958.D (-) m/z 73.10 100.00% 73 I

267 V 355 "T l-l-r-rrT-TT 11.6011.80 12.0012.20 45 133154 193 m/z 267.00 29.42% 0 •n/z-> . 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 7&

355 267 \ 'c ™il ■h 11.60 11.80 12.00 12.20 m/z 355.00 18.36% 45 0 , , . .. rn/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

11.60 11.80 12.00 12,20 m/z74.10 8.91% 5000 267 355 45 I 96 1?3 165 '*^ 223 24/1 293 323 t 0 26 ■n/z-> 50 100 150 200250 300 350 Abundance #362614: Benzeneethanamine. N-[(pentafluorophenyl)methylen... 7)3 ..... .Ij...... 11.60 11.80 12.00 12.20 m/z 268.00 7.11%

5000 267 44 104 131151 179 237 0 ■n/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

6958.D 5080402BBC.M Mon Apr 22 11:42:00 2002 Page 3 .

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