GCMS blank analysis results, sample AE06090, April 2002

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Library Search Compound Report

. Data File C:\MSDCHEM\1\DATA\040402B\LBJ0404.D Vial: 10 Acq On 5 Apr 2002 5:01 am Operator: Bohlk Sample LB 3/15/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Cyciopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 1.25 ug/L 617338 Naphthalene-d8 12.93

Hit# of. 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 52 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 38 4 2,S-DIHYDROXYBENZOIC ACID 3TMS $... 370 C16H30O4Si3 003782-85-2 38 Abundance Scan 1514 (11,975 min): LBJ0404.D (-) m/z 73.10 100.00% 73 1 Tirol 267 355 11.60 11.80 12.00 12.20

m/z-> 0 44+ 118 154 193 237 50 100 150 200 250 300 350 400450500 550 323 JL m/z 267.00 2771^

Abundance #313065: Cyclopentasiloxane, decamethyl- 73

553 267 -p*- 11.60 11.80 12.00 12.20 355 m/z 355.00 19736%

103133163^3223 । 323 0 ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyciopentasiloxane, decamethyl- 73

355 I'i'eo it80 12.00 12’20 267 m/z74710 8.07% 5000

I , 207 323 0 ’p p ' ' ' I Tl/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen.., .... 7)3 355 11.60 11.80 12.00 12.20 m/z 356.00 6.20%

5000

0 4.50 100117147177207 251281- 386 458 P ' I 1 I ■n/z-> 150 200 250 300 350 400 450 500 550 11.60 11.80 12.00 12.20

jBJ0404.D 5080402.M Fri Apr 05 06:26:04 2002 Page 4

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