GCMS blank results, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\LBA0410.D Vial: 12 Acq On : 10 Apr 2002 11:07 pm Operator: Bohlk Sample : LB 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.92 1.58 ug/L 191450 Naphthalene-d8 12.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 86 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 3 1,2-BIS(TRIMETHYLSILYOXY)-4-TRIM. .. 356 C16H32O3Si3 000000-00-0 43 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H22O3Si2 003789-85-3 33 Abundance Scan 1505 (11.922 min): LBA0410.D (-) m/ z 73.10 100.00% 73

5000

267 355

m/z-> 0 I , 'I ' ' 50 100 150 200 250 300 I 350 11.60 11.80 12.00 12.20 m/z 267.00 27.44%

Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 11.60 11.80 12.00 12.20 m/z 355.00 16.05% 45 ■n/z-> oi -V 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl-

11.60 11.80 12.00 12.20 TiTiTil m/z 74.10. 9.33% 267 355 45 26 ,1 I 96 ,133 165, 223 247 i 293 323 0 ' ' 'I ' ' r '' I ' ' 1 I ' Tl/2-> 50 100 150 250 300 200350 Abundance#302821: 1 2-BIS(TRIMETHYLSILYOXY)-4-TRIMETHYLSILYLOXYMETH 7)3 11.60 11.80 12.00 12.20 m/z 356.00 6.49%

553 179 151 209' 267 356 295 319 0 r-A- m/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

LBA0410.D 5080402BB.M Mon Apr 15 16:45:56 2002 Page 4

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