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GCMS analysis results, sample AE06264, April 18, 2002

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Gas chromatography-mass spectrometry analysis of sample AE06264 performed April 18, 2002, detecting unknown compounds and 2,4-DDD surrogate standard.

NYC-WTC_000060076–000060084

Folder label: “GCMS X 3/15/02 A 4/5/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6264 .D vial: 20 Acq On 5 Apr 2002 11:04 am Operator: Bohllc Sample SAMPLE 6264 3/15/02 Inst Instrumen Misc :■ Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASB\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 0.92 ug/L 524557 Naphthalene-d8 12.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 3 Benzeneacetic acid, .alpha.,4-bi... 384 C17H32O4Si3 037148-64-4 37 4 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRI. . . 573 C24H51NO5Si5 000000-00-0 32 Abundance Scan 1514(11.975 min): 6264.D (-) m/z 73.10 100.00% 73

5000 267 355 '' I' UJOItSO 12.00 12.20 125 IM ,193 223 J , 323 I m/z 267.00 26.77% 0 'l6o 150 200 ’ 250“^ Tl/2-> 50 300 350 400 Abundance #313065: Cyclopentasiloxane, decamethyl- 7!3

5000 267 n 11 60 11.80 12.00 12.20 355 m/z 355.10 18.00%

0 , T50 I 96 133 165? ^^ 223244 293 323 ■n/z-> 100 150 200 250 300 350 400 Abundance #313068: Cyclopentasiloxane, decamethyl- 713

355 11.60 11.80 12.00 12.20 267 m/z 74.10 6.77% 5000

45 .207 „ 323 0 I I Tl/Z-> 50 100 150 200 250 300 350 400 Abundance #322334: Benzeneacetic acid, .alpha.,4-bisKtrimethylsilyl... \| 73 267 ■p 11.60 11.80 12.00 12.20 m/z 268.00 6.04%

5000

45 147 341 0 , , 105126 168, ^^3214237 296317 L 369390 1 Tl/z-> 50 100 150 200 250 300 350 400 11.60 11.80 12.00 12.20

.264.D 5080402.M Fri Apr 05 17:16:52 2002 Page 3

NYC-WTC_000060083

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NYC-WTC_000060083Source: NYC Law Department, mirrored locally

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