GCMS analysis results for sample AE06960, April 23, 2002

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Library Search Compound Report

• Data File : C:\MSDCHEM\l\bATA\041702\6960.D vial: 14 Acq On : 17 Apr 2002 7:26 pm Operator: Bohlk Sample : SAMPLE 6960 3/25/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.93 2.94 ug/L 322125 Naphthalene-d8 12.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl-. 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 40 4 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 37 Abundance Scan 1506 (11.928 min): 6960.D (-) m/z 73.10 100.00% 73

5000 267 355 11.60 11.80 12.00 12.20 45 108 154 237 , 323 [ m/z 267.00 28.66% 0 I '• ■' ' ' I ' " •' ' ' I ' ■ ■n/z-> 50 100 150 200 300 250 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 70

5000 267 11.60 11.80 12.00 12.20 355 m/z 355.00 18.23% 45 0 ■n/z~> 50 100 150 200 ' 250 ' 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 .......... ,, I,,( ..................

355 11.6011.80 12.00 12.20 267 m/z 74.10 9.43% 5000

45 207 0^ A-v 50 100 ' 150 I ' 200 ' ' r’’ r-Y-r- ' ■n/z-> 250 300 350 Abundance . #302654: Pentasiloxane, 1.1,3,3,5,5,7.7,9.9-decamethyl- Tb 267 11.60 11.80 12.00 12.20 m/z 356.10 7.34%

. 133 5000 341 207

■n/z-> 0 Y 50 103 100 150 200 , 237^^ 250 300 350 i 11.60 11.80 12.00 12.20

5960.D 5080402BBC.M Mon Apr 22 11:50:14 2002 Page 3

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