GCMS analysis results, Sample AE08264, April 22, 2002

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GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048355–000048377

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 12 Phenanthrene-dlO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.52 ug/L 937329 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 93 2 Anthracene-diO- 188 C14D10 001719-06-8 91 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 53 4 Cycloheptanone, 4-phenyl-188 C13H160 067688-28-2 50 Abundance Scan 3420 (23 174 min): 08264.D (-3413) (-) m/z 188.10 100.00% 188

5000 ) t 94 ' ' l 42 57 66 80 22.80 23 00 23 20 23.40 23.60 122 132 146 158 180 .. 0 mmh- PIIPPNIWT—HTTtn Tron m/ Z 189.15 17.61% Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22 80 23 00 23 20 23.40 23.60 80 m/z 94.10 16.76% 94 160 30 42 52 J 102110118 132 146i il 170 180li | 0 ............... .. 1 ■ ■ ■!<I ■ 'I ■ 11. । ■ H 1rt+Ttttmumgoun TTTunnni n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d10- 188

22.80 23.00 23.20 23.40 23.60 5000 m/ z 184.10 16.19%

80 94 66 160 , । 17 30 42 52 11102 118 132 1114179.189hi7.n7 n 146 Qi................. 'I'...................... l ■ i h P ■ 11 TTTtt 111 ■ I"111 11 >I■ 111"111" 11 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821 Selenide, ethyl 1-methyl-1-penten-3-ynyl 188 1 ‘Tum I 1 1 ' 1 1 1 22 80 23.00 23.20 23 40 23 60 m/ z 80.00 12.00% 5000 79 159 — 145 173 ........................I 91 107 119 131 0 Itt‘1‘1111111111031111111111‘3173 TTTTTITTTTTTTTTTTTTT’ | ‘ l ' i 1 1 ' ‘l ' ‘ IIH Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23.00 23 20 23.40 23.60

08264.D 041702SCAN.M Thu Apr 18 09:52:46 2002 Page 17

NYC-WTC_000048375

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