GCMS analysis results for sample AE08064, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08064 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046757–000046770

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020415\08064.D Vial: 21 Acq On 16 Apr 2002 3:10 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.18 0.47 ug/L 645195 Phenanthranene- dl 0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Phenanthrene-dl0 188 C14D10 001517-22-2 93 Anthracene-dlO- 188 C14D10 001719-06-8 93 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Antipyrine _________________________ 188 C11H12N2O 000060-80-0 38 Abundance Scan 3420 (23 174 min): 08064 D (-3414) (-) m/z 188.40 100.00% 188

5000-

— 80I 94 160 22 80 23 00 23 20 23.40 23.60

n/z-> 0- 42 57 66 । I ' " ' I ' rn | l " I | 11 1 1 rerrpete I 11 i 11 | ri l 11 | > | I '' 'I" ” 1' ’ I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —. 4 I'' "I m/ z 94.30 16.94% Abundance #79827 Phenanthrene-d10 18 8

5000 22'80 23.'oo' 23.20 ’23'40 23.60 80 m/z 189.35 14.14% 94 160 30 42 52 66 102110118 , 132 . । 146 . H, 170 189, O-Tp PHptH TT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d10- 188

22 80 23 00 23 20 23.40 23.60 5000 m/z184.30 12.71%

R 80 94 160 17 30 42 52 ° I | 102 118 132 146 | 170 180 0 17111/1 pri i-» 1111111 n H 11 pt 111111111 h 111111111111 ir < 111111111 h PTi t .......... . 11111 Hr 11' /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771 3-Amino-4-methyl-6-methoxyquinoline ' 1 11 ■ ■ । ■ ■ ■ ■ । ■ 18 8 22 80 23 00 23 20 23.40 23.60 m/ z 80.30 12.19% 145 5000

41 51 63 77 89 102 117 130 159 173 /z—> 0 -------- I rll- l l r. 1 1 1 | All, I 1 rllo । I | I1! I tpr 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I 22.80 23 00 23 20 23 40 23 60

08064.D 041202SCAN.M Tue Apr 16 13:53:54 2002 Page 9

NYC-WTC_000046769

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