GCMS analysis results for sample AE09330, May 8 2002

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Laboratory report documenting GCMS analysis of sample AE09330 conducted on May 8, 2002.

NYC-WTC_000044607–000044620

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9330.D Vial: 10 Acq On 2 May 2002 6:58 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak- Number 7 2-Iodoethyl laurate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.38 0.27 ug/L 337218 Chrysene-dl2 30.82

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Iodoethyl laurate 354 C14H27IO2 1000117-50-2 12 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 12 3 6-Nitro-2-methylpyrrolo[2,3-g]qu... 227 C12H9N302 1000071-35-1 10 4 8-Nitro-2-methylpyrrolo[3,2-F]qu... 227 C12H9N302 072793-30-7 10 Abundance Scan 4818 (31.388 min): 9330. D (-4812) (-) m/z 227.20 100.00% 217 149

5000 113 41 57 167 AA 1 ' i 1 1 ' 1 i ' ' । 84 207 31.00 31.20 31.40 31.60 31.80 ..... ■ '111 । ......... ।11 ■ ■ । । ■ ■ ■ * । ■ ■ ■ ■ । > I I I I I I I I I I I I I I I I I m/z 149.10 70.63% 1’ 1 ' 1 1 11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #89029: 2-lodoethyl laurate 217 43 155 5000 ■I 11 ' ' I ' ' 1 i ' 1 31.00 31.20 31.40 31.60 31.80 m/z 113.50 32.57% 71 97 mlz-> 2 111, " 1117'11' > । । p । .T| 111" 11* ■ ' I ' ' ' ' | ' 40 60 ' ■ | ' ' 183 200 80 100 120 140 160 180 200 220 240 260 280 300 320 340 1111111811111111111111110311 — 354

Abundance #123456:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl)... 149 1.... 1 ll..... i | r l > > | । I ' I ] < । I । | I । i I | r I

31.00 31.20 31.40 31.60 31.80 5000 m/z 167.00 23.54% 70 167 A 41 112 93 | T’TT TH 279 i । | । I । 1 ] i । i । | i i i । [ । i ■ r | I i i i | i i I । | i r > r | t i t T1 1 1 ' | 1 1 1 1 1

/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #89088:6-Nitro-2-methylpyrrolo[2,3-g]quinoline ■ i 1 1 1 1 I ' l > l > > j 1 1 217 31.00 31.20 31.40 31.60 31.80 m/z 228.20 20.63%

5000 181

m/z-> 1 1'11 1 ‘ 11 I 40 60 69 ,1.84, 154 | 197 ■ ■ ■ i ■ I ■ • । • 1 r ' " I " " I....... I I r I < f I > I ' I 1 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ' I 1 1 ' ' I ' 1 31.00 31.20 31.40 31.60 31.80 ' 1 I 1 1

9330.D 050102.M Mon May 06 13:55:12 2002 Page 10

NYC-WTC_000044619

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NYC-WTC_000044619Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE09336, May 2002 · Box DEP Box 25

NYC-WTC_000044708

Laboratory report documenting GCMS analysis of sample AE09336 conducted on May 8, 2002.

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