GCMS analysis results for sample AE09330, May 8 2002

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Laboratory report documenting GCMS analysis of sample AE09330 conducted on May 8, 2002.

NYC-WTC_000044607–000044620

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9330.D Vial: 10 Acq On 2 May 2002 6:58 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00' MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.61 ug/L 828430 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 93 2 Anthracene-dlO - 188 C14D10 001719-06-8 86 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 38 Abundance Scan 3410 (23.115 min): 9330.D (-3403) (-) m/z 188.10 100.00% 188

5000

80 94 1 1 i 1 ' i i-1 । > । । l । T 22.80 23.00 23.20 23.40 40 57 66 111! i > ।! i > 11 > 111 ]'Hi । 1111'Pi 11 > 11 111 : > 104 # TTTT 132.145 12 ll m/z 94.05 18.62% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 I I I I I I I P I A I I I I I — I > I I r

22.80 23.00 23.20 23.40 m/z 189.10 15.38% 80 94 160 30 42 52 66 11 । । । । i । r i i i j i i i i । I । i । । I I । i ] i I I r । । r r । i i ! | | 11 108 118 111111' i' 132 । । i i । । | I । i r। r 146—+4170179— m/z-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 1 ' i 1 1 ' 1 । ' t ' 1 1 1 i• 22.80 23.00 23.20 23.40 5000 m/ z 80.10 12.97%

17 30 42 52 66 6° 80 , 94 , 160 108 118 132 146, 1 I I I [ I I I I I I I I I I I I I 11 I 11 I I I I I I I 11 I I [ I I I I 11 I I 11 I I I I I I I I I j I I I I I I I I I I I #.,179179. TT’T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 11 188 22.80 23.00 23.20 23.40 m/z 184.10 12.13% 145 5000

41 51 63 77 89 102 117 130 ------ Pi 11 rll’ । rRryr 111' " 11 159 173 II /z-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9330.D 050102.M Mon May 06 13:55:11 2002 Page 9

NYC-WTC_000044618

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Laboratory report documenting GCMS analysis of sample AE09336 conducted on May 8, 2002.

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