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GCMS analysis results, sample AE12323, June 2002

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Gas chromatography mass spectrometry results for sample AE12323 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014281–000014302

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document J ~p/U-IU A\ML

Data File : C:\MSDCHEM\1\DATA\052902\12323.D Vial: 11 t Acq On : 29 May 2002 6:14 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 13 Phenanthrene-diO Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.29 ug/L 285470 Phenanthranerie-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# 1 Phenanthrene-diO 188 C14D10 001517-22- 94 2 Anthracene-dlO- 188 C14D10 001719-06-___- 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3401 (23.062 min): 12323.D (-3392) (-) m/z 188.10 100.00% 188

5000 -- 80 94 49 66 160 22.80 23.00 23.20 23.40 0- mm-mHHmmmHm m/ z 94.00 17.80% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

5000 ......... ........................... .. t , 22,80 23.00 23.20 23.40 80 94 m/z 80.00 14.21% 160 30 42 52 66 , 1108 118 132 146 11 170179 0 TIWTNTITTTTTTTTTTTH tretj 11 ■ 111111111 ■ 1111111111.11 > ।HTTT miz-> 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190 Abundance #79826: Anthracene-d10- 1(8 - •1 ____________ 1111 • ‘ i ■ •1 ■ i11 22.80 23.00 23.20 23.40 5000 m/z 189.10 13.88%

ee 80 94 160 , , 17 30 42 52 66 108118 132 146 ,|.| 170179..I 0 T\*HtH nfe-> 10 2030405060 70 8090 100110120130140150160170180190 ........... ............................. Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 188 22.80 23.00 23.20 23.40 m/z 184.10 13.40% 5000 102 115 145 51 63 75 130 158

n/z—> 0------------- '"J1.. on 1111" 11" " i ■ 10 2030405060 70 8090 100110120130140150160170180190 ..0 .. \ .......................... 22.80 23.00 23.20 23.40

12323.D 052202.M Mon Jun 03 10:51:02 2002 Page 16

NYC-WTC_000014301

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NYC-WTC_000014301Source: NYC Law Department, mirrored locally

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