Gas chromatography mass spectrometry results for sample AE12323 including surrogate recovery data analyzed on June 7, 2002.
NYC-WTC_000014281–000014302Folder label: “GCMS X 5/24/02 A 5/29/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document X MUpVuII L\SpUL
Data File : C:\MSDCHEM\l\DATA\052902\12323.D Vial: 11 Acq On : 29 May 2002 6:14 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Bitoscanate Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.26 ug/L 259815 Phenanthranene - dl 0 22.91
Hit# of 5 Tentative ID MW MolForm CAS# Qua
1 Bitoscanate 192 C8H4N2S2 004044-65-9 52 2 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 47 3 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 42 4 Bitoscanate 192 C8H4N2S2 004044-65-9/40 Abundance Scan 3311 (22.533 min): 12323.D (-3305) (-) m/z 192.05 100.00% 19/2
5000
146 160 ......... ...... I ‘*I***I*1*11*.1"I 42 54 66 82 96 22.20 22.40 22.60 22.80 0 ■. ।.. i > |. 11 > n 11111111111’| 111111 r l > |-n > 11111111 I 11111111111 < i > । > ■ 11111 -HHTH h m/z 146.10 22.57% miz-> 0 1020304050607080 90100110120130140150160170180190200 Abundance #125828: Bitoscanate 19/2
5000 ,A 22.20 22.40 22.60 22.80 134 m/z 191.10 21.30% 160 , 50 63 75 90 102 12 148 176 0-nrprooe TTTmmphpm m/z—> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate 192
64 22.20 22.40 22.60 22.80‘11 5000 m/z 193.00 16.34%
39 50 75 90 134
mfe-> 4 0 TIm +18.48+4++H4 14+4/1 it lr# 148 160 TIWTTTTTTTTTTTTTTT 0 1020304050607080 90100110120130140150160170180190200 197.117771/4 Abundance #80999:5H-Dibenzo[a,d]cyc!oheptene 1 ' i 1 1 1 1 1 1 1 i ' ' ‘ ‘ I ‘ ‘ 192 22.20 22.40 22.60 22.80 m/z 160.00 12.16% 177 5000
165 89
m/z—> 39 51 63 76 ,102 115 128139> 152 0 TTTTTTTTTTT*T**TTpttt’t Trn- 0 1020304050607080 90100110120130140150160170180190200 m 447447.— 1 1 I ‘ ■ 22.20 22.40 22.60 22.80 1
12323.D 052202.M Mon Jun 03 10:51:01.2002 Page 15
NYC-WTC_000014300
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NYC-WTC_000014079
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12473 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014330
Gas chromatography mass spectrometry results for sample AE12325 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014260
Gas chromatography mass spectrometry results for sample AE12322 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014102
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12474 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014237
Gas chromatography mass spectrometry results for sample AE12321 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014054
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12472 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014189
Gas chromatography mass spectrometry results for sample AE12288 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014214
Gas chromatography mass spectrometry results for sample AE12320 including surrogate recovery data analyzed on June 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023949
Laboratory report showing GC/MS analysis of sample AE10983 with surrogate recovery data for 2,4-DDD.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024167
Lab notes regarding low recovery in sample AE10206 requiring re-extraction and successful re-analysis on May 21, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025304
Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11415 conducted on May 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023887
Laboratory report showing GC/MS analysis of sample AE10980 with surrogate recovery data for 2,4-DDD.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000014149
Laboratory log listing the sequence of samples and calibration standards processed by GCMS on May 24 and May 28, 2002.
Filed in the same folder
NYC-WTC_000014150
Fragmented document header from the DEP Box 15 archive containing metadata for environmental testing records dated late May 2002.
Filed in the same folder
NYC-WTC_000014154
Laboratory report documenting gas chromatography-mass spectrometry analysis of a method blank (AE12288) for volatile organic compounds on June 3, 2002.
Filed in the same folder
NYC-WTC_000014177
Calculated reference values and recovery percentages for organic compound analysis using gas chromatography-mass spectrometry with all results at or above 2.0 ug reporting limit.
Filed in the same folder
NYC-WTC_000014185
Laboratory report showing reference calculations for volatile organic compounds in sample AE12288 analyzed on June 3, 2002.
Filed in the same folder