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GCMS analysis results for sample AE11419, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11419 conducted on May 30, 2002.

NYC-WTC_000025414–000025429

Folder label: “GCMS X 5/16/02 A 5/20/02

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Scanned page image, NYC-WTC_000025425
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11419.D Vial: 9 Acq On : 20 May 2002 7:48 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Bitoscanate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.24 ug/L 247712 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Bitoscanate 192 C8H4N2S2 004044-65-9 53 2 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 42 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 42 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 Abundance Scan 3318 (22.574 min): 11419.D (-3312) (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.20 22.40 22.60 22.80 23.00

m/z-> 0 TTTTTTLTTTTTTTTTTTTHWTTTTTTT 52 70 | J 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I'1111 " 111 A.# I'11' I — m/z 191.10 17.41% Abundance #125828: Bitoscanate 192

- 5000 22.20 22.40 22.60 22.80 23.00 134 m/z 146.10 16.50% 90 160 50 63 75 I .102 miz-> 0 -+ +--H 1H 122 IT +THm 176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 148

Abundance #81041: Phenanthrene, 3-methyl- 192 "I -4 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 16.01%

96 27 39 51 63 82 II 115 126 139 152 165 176 0 I P I I I P I I l‘p I I I P I I I p’l I l P I’l l pl I I I I I I I I |'i Tt i | । 1 I i | I i ■ i'p I i > |'l i i i | l'l'l i | । ill | i > i'l'

mlz-> 20 30 40 50 60 70 80 90 100,110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 1 i 1 1 ■ ■ i ' ■ ' ■ i ' 192 22.20 22.40 22.60 22.80 23.00 m/z 160.10 11.87%

5000

96 1 cE

m/z-> 27 39 51 0 TIWWTIWITIOIImmmmuuuupr 63 82 ll 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 115 126 139 152 190 178 U 22.20 22.40 22.60 22.80 23.00

11419.D 050102.M Thu May 23 10:46:55 2002 Page 7

NYC-WTC_000025425

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NYC-WTC_000025425Source: NYC Law Department, mirrored locally

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