GCMS analysis results, sample AE12323, June 2002

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Data File : C:\MSDCHEM\l\DATA\052902\12323.D Vial: 11 Acq On : 29 May 2002 6:14 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 1,3-Dioxane-2-propanol, 2-m... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 7.72 0.21 ug/L 133405 11 4 -Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MblForm CAS# Qual 1 1,3-Dioxane-2-propanol, 2-methyl- 160 C8H16O3 036651-31-7 1 2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 9 3 3-Pyrrolidinol 87 C4H9NO 040499-83-0/9 4 2-Butanol, 3-methyl-, acetate 130 C7H14O2 005343-96-/ 9

i Abundance Scan 789 (7,715 min): 12323.D (-783) (-) m/ z 43.1010y.00% 43

5000 WMMwt 58

+ 87 35 51 98 —• i ■ ■ ■ 1 i 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i

m/z-> 0- -H 20 30 40 50 60 70 80 1 90.100 110 120 130 140 150 -n-p-r-r-r-p- - m/z 7.40 7.60 58.00 7.80 8.00 29.19% Abundance #5776:1,3-Dioxane-2-propanol, 2-methyl- 43 58

5000 7.40 7.60 7.80 8.00 84 m/z 87.10 24.37% I 69 O-rri I I T| ■ I M |' - ITT 1'101 i'1 • ‘ ■ i4 ‘ ■ i ■ ‘ ' i ■ ■ ■ • i • 145 ■ i ■ • mfa-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #110033:4-Penten-2-one, 4-methyl- 43 ■ ■ ■ 1 i ■ ■ ■ ■ i ■ ■ 1 ’ r 7.40 7,60 7.80 8.00 5000 m/z 84.00 16.84%

0- 28

...lIilh 55 ----- 98 83 MMwwkoua miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4163:3-Pyrrolidinol T 43 7.40 7.60 7.80 8.00 m/z 35.10 16.36% 5000 h N 87 57 68 0 11111' I ''1' i -H — It T n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.40 7.60 7.80 8.00

12323.D 052202.M Mon Jun 03 10:50:59 2002 Page 14

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