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GCMS blank analysis results for volatile organics, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.

NYC-WTC_000023409–000023423

Folder label: “GCMS X 5/9/02 A 5/13/02

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Scanned page image, NYC-WTC_000023420
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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\051302\0506LB.D Vial: 6 Acq On : 13 May 2002 3:33 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.38 ug/L 458698 Phenanthranene-dl0 22.95

Hit# of

1 Phenanthrene-diO 5 Tentative ID MW

188 C14D10 MolForm CAS# 001517-22-2 5900/ oualM 2 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 53 Y 3 Anthracene-d10- 188 C14D10 001719-06-8 47/ / 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3409 (23.109 min): 0506LB.D (-3404) (-) m/z 188.10 100.00% 1518

5000 ....... .... ........................... 94 22.80 23.00 23.20 23.40 . /in 59 OA 66। 160 80 । 0t | I । I । | ITTTT HTHTH '11'" ' I " " I" '11 ----- m/ z 94.05 14.74% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/Z 184.10 12.33% 94 80 -160 30 42 52 66 , ,| 108 118 132 146 ,|, 170179,,| 0 1111" ।। 1111'" 11 i ।! 11111111! ii 11 TTTTTTTTTTPTT IT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline US

22.80 23.00 23.20 23.40 145 5000 m/z 189.10 9.48%

117 41 51 63 77 89 102 130 159 173 I | I I r11■p-m-r ■■■'i1!....... r'" 0- I | I I I I | I I I I | I I I I ‘ I rlrr rlli’n | । ill- I l rl’r- । I j'l'l-l I | I rill. I I r-nT |‘l Pl | I ......... . m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1tS 22.80 23.00 23.20 23.40 m/ z 66.20 7.78%

5000

. 80 94 160 , | 17 30 i ii 42 52 66 , 1 108 118 132 146.,.479179 T’IUIT 0 ' i " "i " " r [ I h 11 I I । । | t l ti [ ri I I 1 1111" I " " I " 1' I" " 11111 rJz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

0506LB.D 050102.M Tue May 14 11:31:59 2002 Page 9

NYC-WTC_000023420

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NYC-WTC_000023420Source: NYC Law Department, mirrored locally

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