GCMS blank analysis results for volatile organics, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051302\0506LB.D Vial: 6 Acq On : 13 May 2002 3:33 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Quinoline, 3-bromo- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.96 0.35 ug/L 223392 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Quinoline, 3-bromo- 207 C9H6BrN 005332-24-1 22 2 Quinoline, 3-bromo- 207 C9H6BrN 005332-24-1 1 3 Quinoline, 8-bromo- 207 C9H6BrN 016567-18-3 / 2 4 2-Chloroaniline-5-sulfonic acid 207 C6H6C1NO3S 000098-36-2 11 Abundance Scan 5426 (34.960 min): 0506LB.D (-5424) (-) m/z 129.30 100.00% 129 207 281 96 261 5000

‘it 4AA4A— 44 34.60 34.80 35.00 35.20 0 i ' 1 ■ 1 i 1 1 i 1 ■ ' ' i ■ ' m/Z 131.00 71.92% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84880: Quinoline, 3-bromo- 128 207

5000 101 . Ilfth, AB..., 34.60 34.80 35.00 35.20 75 m/ z 2 81.00 69.40% 50 26 38 h 62 141153 181, 0 I 11 1 1 1 1 L m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #126483: Quinoline, 3-bromo- 128 207 ■ * । * 1 * । ■ 34.60 34.80 35.00 35.20 5000 101 m/z 207.00 68.45%

m/z-> 50 75

26 38 163 118711 | nr 141 155 0 1’11 17 1। | i 1f 11" Ri 20 40 60 ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । 80 100 120 140 160 180 200 ■ i ■ 181 220 240 260 280 wpllyonnphb** Abundance #84881: Quinoline, 8-bromo- 128 207 34.60 34.80 35.00 35.20 m/z 95.90 58.68%

5000 101 50 64 0 -T" +189—4— 115 26 38 || . 142154 171184 1 ■ r11 1 Im 1 r1'1 ■11 ■ — — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

0506LB.D 050102.M Tue May 14 11:32:01 2002 Page 10

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