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GCMS blank analysis results for volatile organics, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.

NYC-WTC_000023409–000023423

Folder label: “GCMS X 5/9/02 A 5/13/02

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Scanned page image, NYC-WTC_000023422
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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\ 1 \DATA\ 051302\050 6LB . D Vial: 6 Acq On : 13 May 2002 3:33 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Glycyl-d-tryptophan Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

35.01 0.28 ug/L 178153 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Glycyl-d-tryptophan 261 C13H15N3O3 1000126-30-0 9 2 .alpha.-Methylstyrene 118 C9H10 000098-83-9 50 3 Benzene, 1-ethenyl-3-methyl- 118 C9H10 000100-80-1 5 4 Benzene, 1-ethenyl-4-methyl- 118 C9H10 000622-979 5 Abundance Scan 5435 (35.013 min): 0506LB.D (-5434) (-) m/z 281.00 100.00% 201 118 133 5000 207 44 262 r। 1 1 1 1 1 ■ ' ' • । 1 1 1 1 i 1 1 34.60 34.80 35.00 35.20 35.40 I 1 11 0000 m/z 118.30 74.92% Ol ' 1 I ' 1 1 ' 1 ■ i 1 1 ■ ■ । ■11 * ।11 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #52554: Glycyl-d-tryptophan 1* 7130

5000 44 1 mTr । । । . 90 34.60 34.80 35.00 35.20 35.40 m/z 115.70 64.58% 63 77 —ll—4l 193441 ! I | 143156 187 243 261 01 ■11' 1 1 1" 1 i’i > i i 1 | Di i i | । । i > -|—r i i i । I i । । |' । i | i | i .

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #120635: alpha.-Methylstyrene 1 8 11 1 1 ' TTp—BBnn/m 34.60 34.80 35.00 35.20 35.40 5000 103 m/z 117.40 57.99% 78 51 27 । Of ' 111''11 r1 r" rdpi in" i" 65 nz-> 120 140 160 180 200 220 240 260 280 Abundance 20 40 60 80 100 #52522: Benzene, 1 -ethenyl-3-methyl- 17 _M 34.60 34.80 35.00 35.20 35.40 m/z 133.00 56.74%

5000 91 J 39 63 77 26 a 1,1 Ji h 104 |! 0 ‘-1/dt/"[/1/"/t/1511*1"1/1111‘1711111-11-11111711111‘111111111111111111171 —LL ■n !l ‘ ‘I Uli Hill HiMR mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20 35.40

0506LB.D 050102.M Tue May 14 11:32:03 2002 Page 11

NYC-WTC_000023422

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NYC-WTC_000023422Source: NYC Law Department, mirrored locally

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