GC/MS results for unknown compounds and surrogates, sample AE10984, May

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Data File : C:\MSDCHEM\l\DATA\051402\10984.D Vial: 13 Acq On : 14 May 2002 11:17 pm Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 2H-3,1-Benzoxazine, 2-[4-(d... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

35.35 0.35 ug/L 343891 Perylene-dl2 ' 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-3,1-Benzoxazine, 2-[4-(dimeth... 260 C16H24N2O 142927-50-2 9/ 2 6H-Dibenzo[a,g]quinolizine, 5,8,... 355 C21H25NO4 002934-97-6/9 3 4a(2H)-Naphthalenecarboxylic aci... 222 C13H1803 007478-39-9 7 4 2-Butenoic acid, 3-(phenylthio)-... 222 C12H1402S 013141-01-0 5 Abundance Scan 5492 (35.348 min): 10984.D (-5490) (-) m/z 263.20 100.00% 43 96 147 2(3 341 193

5000 __ 222 295 "184 ■ ■ l ■ > > > I ■ I l 1 > < I I 429 35.00 35.20 35.40 35.60 L I

A 0- m/z 147.10 94.44% niz-> 50 100 150 200 250 300 350 400 Abundance #66585: 2H-3,1 -Benzoxazine, 2-[4-(dimethylamino)phenyl]oct... 148

5000 _AC L 35.00 35.20 35.40 35.60 260 m/z 43.10 91.20% 187 230 01 41, il 77 100 121 Ah 4 4 L 4-+— m/z-> 50 100 150 200 250 300 350 400 Abundance #123506: 6H-Dibenzo[a,g]quinolizine, 5,8,13,13a-tetrahydro... 149 355 35.00 35.20 35.40 35.60 5000 m/ Z 95.90 90.28% 190 77 121 324 0- 51,,1 92,4 .> 220 250 280 304 T—*I—t — ■n/z-> 50 100 150 2001 250 300 350 400 Abundance #66990:4a(2H)-Naphthalenecarboxylic acid, 1,3,4,5,6,7-hex... 149 ■ ‘ T ’ 1 35.00 35.20 35.40 35.60 1 ■ ‘ i '

m/z 341.10 90.28% 107 5000 29 79 222 55 0 1 .i 1 i 149 175194 1 ...... ........ ........ ■ > i ■ ■ ■ > i - ■ ■ ■ i । ■ i ■ miz-> 50 100 150 200 250 300 350 400 35.00 35.20 35.40 35.60

10984.D 050102.M Thu May 16 14:41:50 2002 Page 17

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