GCMS blank analysis results, sample AE10809, May 2002

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Data File C:\MSDCHEM\1\DATA\051402\0507LB.D Vial: 16 Acq On 15 May 2002 2:34 am Operator: Mclean Sample 5/7 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 16 3-Benzofurancarboxylic acid... Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

35.42 0.31 ug/L 140911 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Benzofurancarboxylic acid, 2-[... 282 C17H1404 040800-98-4 9 2 2-Oxo-4-phenyl-6-(4-chlorophenyl... 282 C16H11C1N2O 024030-13-5 3 2(1H)-Pyrimidinone, 5-chloro-4,6. . . 282 C16H11C1N2O 028567-83-1 5 4 IIH-Dibenzo[b,e][1,4]diazepin-11... 281 C17H19N3O 013450-70/9 5 Abundance Scan 5504 (35.418 min): 0507LB.D (-5495) (-) m/z 147.10 100.00% 147

5000 73

96 221 281 355 yMMW" 44 n . i r — rT , . 191 35.00 35.20 35.40 35.60 35.80 0- i111' 111111 ......... I.......... i ‘' r 111 i'''' i r j 1 । । । । > । : > । । । । । । r। । । । । । । । m/z 73.10 68.87% n/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240_260_280_ 300 320 340 #87976: 3-Benzofurancarboxylic acid, 2-[(2-hydroxyphenyl)m... 221 250 J 282 5000 165 35.00 35.20 35.40 35.60 35.80 m/z 221.05 62.26% 44 194

ph“W 77 97 139 0-mPT 11— —1| 11111'' I i11'■।'1111' > > ■ । ■ 11 ।11 ■ ■ ।1 11 ■ । 1 ti/z—>40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #97369: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrim... 281 TT 35.00 35.20 35.40 35.60 35.80 5000 m/z 3 55.00 59.37%

3,6 52 77 102 123 141 175 204 247 01- TTTmmgtn TT r 11' i -P T1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #97366: 2(1 H)-Pyrimidinone, 5-chloro-4,6-diphenyl- ‘‘‘‘I’’ ' i 1 ■ ■ ■ । 1 1 1 1 281 35.00 35.20 35.40 35.60 35.80 m/z 281.05 56.34%

5000 77 104 ill!..........ii 204 247' 1 Mak" O—TTTT ■ ■ i'111 111111 TPTTHTP ’' 111 11 11 r 1 ' 1 r 1 ■ 11 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.00 35.20 35.40 35.60 35.80

0507LB.D 050102.M Thu May 16 12:36:02 2002 Page 19

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