GCMS analysis results for sample AE11382, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11382 conducted on May 22, 2002.

NYC-WTC_000025127–000025144

Folder label: “GCMS X 5/15/02 A 5/17/02”

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NYC 9/11 Public Portal Document Llbrary Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11381.D Vial: 8 Acq On : 17 May 2002 6:29 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 3-Benzofurancarboxylic acid... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 33.08 0.20 ug/L 170195 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 3-Benzofurancarboxylic acid, 2-[... 282 C17H1404 040800-98-4 12 2 Pyrazolo[1,5-a]pyridine, 3,7-dim... 222 C15H14N2 017408-36-5/12 3 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 1000124-33/0 9 4 3-Buten-2-one, 4,4-diphenyl- 222 C16H14O 000837-66/1 7 Abundance Scan 5106 (33.080 min): 11381 .D (-5098) (-) m/Z 221.10 100.00% 73 221 355

148 282 429 5000 ■ 1 ' i ' ' IIIIIIIt 1 ■ i 1 ' 49 32.80 33.00 33.20 33.40 o- ‘' r 1" i" " i" " 1 " 11'" ■ i' ■ ‘' I" " i" " i" “ i ■ ■ ■ m/z 355.00 92.53% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #87976: 3-Benzofurancarboxylic acid, 2-[(2-hydroxyphenyl)m... 221 250

5000 165 282 1 i ' ‘ Ifi Im 32.80 33.00 33.20 33.40 ' 1 i ' 1

44 m/z 73.05 85.39%| 1 77 97 139 194 01 I 11 I I | l '« । l * । 1 ’ | * r, . j , LLL L , 11 , I ,, , I I TTT - /z-> 40 60 80 100120140160180200220240260280.300320340360380400420 Abundance #87872: Pyrazolo[1,5-a]pyridine, 3,7-dimethyl-2-phenyl- 1 9 22!1 L 32.80 33.00 3320 33.40

5000 m/z 148.10 64.61%| 51 92 145

miz-> 0 ll " i" " i '111 1’’’’0’110T"011118191T"I"0—10103—U—0T3I011111 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #87894:1,3-Benzodioxole, 5-[3-acetaminopropyl]- ' 1 I ' 1 1 1 I ■ ■ 1 I ' 1 1 1 I ' ' 221 32.80 33.00 33.20 33.40 m/z 83.90 64.29% 135 162 43 73 5000 fl A w 1 91 0V — +4 44— 1 17.+, 192 T—TTTpTTTTTTTTTTTTTTTTTTTTTTTTT i" “ i m/z-> 40 60 80 100120140160180 200220240260 280 300 320 340 360 380 400 420 32.80 33.00 33.20 33.40

11381.D 050102.M Tue May 21 14:25:33 2002 Page 10

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GCMS analysis results for sample AE11381, May 22 2002 · Box DEP Box 18

NYC-WTC_000025102

Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.

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