DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Llbrary Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02454 .D Vial: 5 Acq On : 27 Feb 2002 6:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 (4-Acetyl-7,7-dimethyl-bicy ... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 38.32 0.13 ug/L 80028 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 (4-Acetyl-7,7-dimethyl-bicyclo [3... 206 C13H18O2 077822-36-7 30 2 (3E)-4-[trans-4’ ,4',5’-trimethyl. . . 206 C14H220 127128-62-5 14 3 Acetamide, N-(2,6-dimethylphenyl)- 163 C10H13NO 002198-53-0 12 4 ethyl 3-(3-hydroxypropyl)benzoat... 208 C12H1603 114837-80-8 11 Abundance Scan 3096 (38.324 min): 02454.D (-) m/z 43.10 100.00% 43 121 93 163 5000 69 145 329 213231 255 396414 193 282 38.00 38.20 38.40 38.60 0- " i1" ■ I'11 i i " !’———1—441t22a19111 —2711*1111/411//1*1117/177**11**’1***317** I' “ 111 m/ z 55.00 78.29% m/z-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #124061: (4-Acetyl-7,7-dimethyl-bicyclo[3.2.0]-1 -hepten-3-.. 43 A 5000 163 . I I, ,l , / 38.00 38.20 38.40 38.60 121 m/z 121.10 . 76.03% 91 206 I ...Illi I I 145 li 0- " i " 1 j " " I ■'1' i'" ' 1" 1111111''' r 111 r " ' r ' " i "1' r 1111" " i" " i" '11 ‘' i1' " r 1 " i1 " 11 ‘ m/z-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #124701: (3E)-4-[trans-4 ’,4’,5’-trimethyl-2’-methylidenecy... 43

163 38.00 38.20 38.40 38.60 5000 107 m/z 57.10 75.01% 83 191 135 ''11 " i" " i1"11" " i"111" " । ।।। ।' 'i ■ | 0-1111111111111101101111111111111111171113 m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #63346: Acetamide, N-(2,6-dimethylphenyl)- 121 38.00 38.20 38.40 38.60 m/z 105.10 69.02% 163 5000 1 77 ......... . ................... . 0 1H "1!" " i" ■ 'r 1"r1"r " 11" " i" " i"1'i " "i" "i " " i" "i' m/z-> 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400 38.00 38.20 38.40 38.60

02454.D HP022102.M Thu Feb 28 08:47:35 2002 Page 15

NYC-WTC_000005104

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NYC-WTC_000005104Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999