GCMS analysis results for sample AE00309, Jan 2002

NYC 9/11 Public Portal Document

Llbrary Search Compound Report Data File C:\MSDCHEM\1\5973N\02JAN08\309.D Vial: 8 Acq On 8 Jan 2002 11:19 pm Operator: Sample 508scan Inst : Instrumen Mise 2002 January 8, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 3-Buten-2-ol, 2-methyl- (CA... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 4.62 0.14 ug/L 44189 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 9/ 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 9 3 2-N-PROPYL-I-DI-AZIRIDINE 86 C5H10DN 030691-56-6 9 4 2-Propyldecan-l-ol 200 C13H280 000000-00-0 9 Abundance Scan 109 (4.618 min): 309.D (-) m/z 41.10 100.00% 41 57 88 71

5000 85 14 47 53 1 lu 4.20 4.40 4.60 4.80 5.00 0 11 ■ ■ ■' i ■''11'11' 11 TT TTT TT 1 f i1 ■ ■ ■ ।111 ‘ i • ■ i ■ ■ ■ > i ■ • ------ rr T ’ ’IT m/ z 57.10 92.67% n/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4090: 3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 43 71

5000 dn 1 ' I ' 1 1 1 f1 ' 4.20 4.40 4.60 4.80 5.00 27 59 31 39 m/ z 88.00 91.90% 0 1111 ■ ■' r "'i11111" T Tmnpuii - ■ i •''11 ■ ■ ■ ■ i' ■ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4083: 3-Buten-2-ol, 2-methyl- 71 43 A_ 4.20 4.40 4.60 4.80 5.00 5000 m/z 71.10 72.64% 59 27 31 53

ti/z-> 0 ■' 111" i' 20 25 TTIf 30 37 'I..... arl +i" " i1 r ) i 1 35 40 45 50 55 60 65 70 75 80 85 90 95 — Abundance #3649: 2-N-PROPYL-1-D1-AZIRIDINE i ' ' ■ ' i 57 85 4.20 4.40 4.60 4.80 5.00 m/z 43.10 66.91% 71 5000 26 31 42

m/z-> 0 TTPUTTTt . ITi 20 25 30 mH 35 40 45 50 55 60 65 70 ■ ■ i11'' i'' 75 80 85 90 95 4.20 AMANW, , 1 1 1 11 IT* ' 1 v I 11 1 1 1 11 ' 4.40 4.60 4.80 5.00

■ 09.D SCAN508.M Wed Jan 09 1-5:17:25 2002 Page 4

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