GCMS analysis results for sample AE00307, Jan 2002

NYC 9/11 Public Portal Document

Llbrary Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 Acq On 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************************************************** k * * *

Peak Number 2 2-Buten-1-ol, 3-methyl- (CA... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

4.62 0.17 ug/L 55291 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-I-ol, 3-methyl- (CAS) $$... 86 C5H10O 0 0 0 5 5 6 - 82-1 62. 2 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 56 3 2-Buten-I-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 56 4 2-Buten-1-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 53 Abundance Scan 109 (4.618 min): 307. D (-) m/z 71.10 100.00% 41 71 57 88 5000

44 53

67 85 4.20 4.40 AN 4 60 4.80 5.00

n/z-> 01 ■ ■ i ■ ■ ■ ■ i1' ■ ■ i ■ ■ ■ ■ i1 ■ 20 25 149+., 30 35 40 45 50 55 60 65 70 75 80 85 90 i ■ ■ ■ ■ । ■ +— ■■I.......... HI 1111'' i1 95 m/z 41.10 95.34% Abundance #4075: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 41 5000 A, , 1 i 1 1 1 . . ........... ... 1 11 1 i ' 1 53 4.20 4.40 4.60 4.80 5.00 86 67 m/z 57.10 68.72%

m/z--> ol • • i ■ • • • । 20 25 ■ 11 30 > i ■ ■ ■ ■ 11 35 40 TTTTT 45 50 55 60 65 ■ r '111' + 83 . ................. ... 70 75 80 85 90 95 Abundance #4069: 2-Buten-1-ol, 3-methyl- 7h ..................................

4.20 4.40 4.60 4.80 5.00 5000 27 39 53 m/ z 88.10 59.55%

31 68 86

m/z-> Ol 1 ■ i ■ ‘ ■ i' 1111 ■1' i ■' I"" .............. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 49 .. 59... .Ill, --rp-r

Abundance #4072: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 4.20 4.40 4.60 4.80 5.00 m/ z 43.05 48.28%

5000 27 39 53

m/z-> 31 49 59 0 TT-pn-rr-p- 7 ' i1" ■ i' ■ I " '1111111 " • i1 ■ ■11 • 20 25 30 35 40 45 50 55 60 68 | 86 ‘i11' 11 - TTT17 65 70 75 80 85 90 95 \ MneA) 4.20 4.40 4.60 4.80 5.00

307.D SCAN508.M Wed Jan 09 15:16:56 2002 Page 4

NYC-WTC_000051062