GCMS results for sample AE00469, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00469.D Vial: 8 Acq On : 11 Jan 2002 7:55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 2-Buten-l-ol, 3-methyl- (CA... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 4.63 0.12 ug/L 47739 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 43 2 2-Buten-I-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 38 3 2-Buten-I-ol, 3-methyl- 86 C5H10O 000556-82-1 38 4 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 32 Abundance Scan 110 (4.630 min): 00469.D (-) m/ z 41.10 100.00% 41 57 71 88 1 5000 53 101 AANN 1 4.20 4.40 4.60 4.80 5.00 o i""i 1 ‘ p'" p TT ■ ■ p "' p ’ ■ p1'r p " ■ । " i1 ■" p m/z 88.00 96.89% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4076: 2-Buten-1 -ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 7h 41 5000 +‘II T 1 53 86 4.20 4.40 4.60 4.80 5.00 27 m/ z 71.10 95.84% 0 ‘II ip■■<। ■ i • 1111 ippppp'”"!' p1 p1 p"■ p" ■ p■1'i' ' p'" p ■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4075: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL...

41 7(1 _A 4 20 4.40 4.60 4.80 5.00 5000 m/z 57.10 86.46% 53 86

m/z-> 0 11 P1" P 11 ‘ p 1 " P 11' l I m —pu 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 " p11' I p " p "' p " 1 p "' i" " p

Abundance #4068: 2-Buten-1-ol, 3-methyl- 1 .......... 71 4.20 4.40 4.60 4.80 5.00 "2 43.10 56.62% 5000 53 27 86

n/z—> 0 " p "' p l p " p p ’ i T —fli 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 1 pp-p-' । 11 p 11P'1 ■ p 11' P n ■ i1 ‘ ■1 p _AAAAN4 4.20 4.40 4.60 4.80 5.00

00469.D SCAN508.M Mon Jan 14 10:47:11 2002 Page 3

NYC-WTC_000051477