GCMS analysis results for sample AE00309, Jan 2002

NYC 9/11 Public Portal Document

Llprary searcn compound Report

Data File C: \MSDCHEM\1\5973N\02JAN08\309.D Vial: 8 * Acq On 8 Jan 2002 11:19 pm Operator: Sample 508scan Inst : Instrumen Mise January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 1-Butanamine, 3-methyl- (CA... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.13 ug/L 40899 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine, 3-methyl- (CAS) $$ . . . 87 C5H13N 000107-85-7 9/ 2 Oxirane, (2-methylpropyl)- 100 C6H120 023850-78-4 9 3 Formic acid, 2-methylpropyl ester 102 C5H10O2 000542-55-2 8 4 Monomethylnitrosamine 6 0 CH4N20 064768-29-2 7 Abundance Scan 76 (4.241 min): 309.D (-) m/ z 85.00 100.00% 85

41 5000

47 60 __ Ml, A—A— 380 4.00 4.20 4.40 4.60 0—— ' i ' ■ 1 ' 1 1 ' ' ■ I I , ■ ' I TTT+ 1 1 I 1 1 ' 1 I 1 ' ‘ ' l I I m/z 41.10 59.46% /z-> 10 20 30 40 50 80 90 100 60 110 70 Abundance #4416:1-Butanamine, 3-methyl- (CAS) $$ Isoamylamine $$ Le... 41

5000 55 70 87 ./MA.,., 3.80 4.00 4 20 4.40 4.60 m/z 43.10 57.09%

Tl/Z--> o1 ' 1 T r ' । ■ | ' r ■ 1 | > > 10 20 30 rT 40 ■ ■ i

50 ■ ■ 11 1 i

60 ■ 1

70 ■ ■ i ■ > > l I ■ ■ ' ' i • ■ ■ ■ i 80 90 100 110 Abundance #8525: Oxirane, (2-methylpropy!)- 85 — M 3.80 4.00 4.20 4.40 4.60 41 55 5000 m/z 39.00 24.22% 29 y 69 -- o1 ■ ■ i ■ ■ 1 ' i ■ ' ' 1 r • ■ 1 ' i ■ ■ । 1 1 1 i 1 1 ■ ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9307: Formic acid, 2-methylpropyl ester — ' ' i 1' 1 r i 1 1 1 1 r 1 43 3.80 4.00 4.20 4.40 4.60 56 m/z 60.10 23.62% 31 5000

15 151 0 ..... I...... LL I 73 102 11 I1 ' ■ ■ i 1 ' i ■ ■ ■ ' । । ■ ■ ■ ' । 1 ■ ■ ■ । 1 ' ■ ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.80 4.00 4.20 4.40 4.60

309.D SCAN508.M Wed Jan 09 15:17:25 2002 Page 3

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