DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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Data File : C:\MSDCHEM\1\5973N\02FEB27\02454.D Vial: 5 Acq On : 27 Feb 2002 6:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ******************************************************** * ** *** * * * *** * Peak Number 12 Hydrazinecarboxamide, 2-(l,... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

36.66 0.08 ug/L 46084 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrazinecarboxamide, 2- (1,7,7-t.. . 209 C11H19N3O 004581-48-0 25 2 Lactone of 5-Acetyl-1,3,3,4,5-pe... 194 C12H1802 059873-44-8 25 3 6H-Purin-6-one, 2-amino-l,7-dihy... 151 C5H5N50 000073-40-5 16 4 6H-Purin-6-one, 2-amino-l,7-dihy... 151 C5H5N50 000073-40-5 16 Abundance Scan 2949 (36.665 min): 02454.D (-) m/z 151.10 100.00% 151

69 5000

41 189 410 91 109

m/z-> 0 1111133 TTT I1111 11" ‘ 111'11'11 ‘ I ‘ '11" +1208, 281 ’1’4411’’1411/’1/*/’1’171111719/1/1117 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 360 380 400 L m/z 36.40 36.60 36.80 37.00 69.10 58.80%

Abundance #128680: Hydrazinecarboxamide, 2-(1,7,7-trimethylbicyclo[2.„ 151

5000 36.40 36.60 36.80 37.00 107 m/ z 81.00 25.32% 44 67 209

m/z-> 0- L ML ..... I I. .................................................. 134 .

40 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #106286: Lactone of 5-Acetyl-1,3,3,4,5-pentamethylbicyclo[... 151 36.40 36.60 36.80 37.00 5000 m/z 150.10 24.42% 194 V 133 91 109 ..........Ill II ll , 0- '' I'1" r " 1T111’1’111 11 ‘ ‘ I’T ' i ‘ ' I" " i “ " r "' i" " I"' ‘ i1"' i " ■' i" " i" 111 ■ ‘" i m/z-> 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #47527:6H-Purin-6-one, 2-amino-1,7-dihydro- 151 36.40 36.60 36.80 37.00 m/z 41.10 23.50% / 5000

53 110

m/z-> 0 IL II 134 i'1 ■ ■ i1" ■ i ■11 ■ i ■" ■ i" " i" " i" " i" ■' i'1" i1'" i" " i" " i" " i' ‘" I" " r'" i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 36.40 36.60 36.80 37.00

02454.D HP022102.M Thu Feb 28 08:47:35 2002 Page 14

NYC-WTC_000005103

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999