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GCMS analysis results for sample AE01440, Feb 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated February 22, 2002.

NYC-WTC_000038623–000038631

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document Llorary searcn compound Keporc

Data File : C:\HPCHEM\l\DATA\FEB2102\1440.D Vial: 12 Acq On : 22 Feb 2002 12:56 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.29 158.77 ug/1 9187560 Perylene-dl2 38.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 2 [1,1'-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 38 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO 000000-00-0 17 4 Pyridine, 4-[4-methoxyphenyl] - 185 C12H11NO 000000-00-0 17 Abundance Scan 3404 (36.289 min): 1440.D (-) 100.00% 185

57 5000 112 83 1 1 1 1 1 143 166 36.00 36.20 36.40 36.60

m/z—> 0+ 444W 203 240 268 297315 340 369 397 426 •n———11—1000——T——m01—0070—0——0—3099U330333-1"3TVT1TTT 40 60 80 100 120140 1601 80 200 220 240 260 280 300 320 340 360 380 400 420 m/ z 57.0,0 51.51% Abundance #55661: Decanedioic acid, bis(2-ethylhexy!) ester 185

5000 - 57 • ■ l • ■ ■ • l 1 ' C ' ' ' 1 1 1 112 36.00 36.20 36.40 36.60 | 83 m/ z 70.1,0 35.92% 143 166 298316 203 "11"'11" TTTh ' “I—I0E0—00mu————n———0Tu1—1TTT TTT | I I I I [ I I I I mc->(40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 185

36.00 36.20 36.40 36.60 5000 m/z 71.00 34.17% 156 128 { m/z->. _. 40. 60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420'' Abundance #19196: Pyridine, 4-[4-methoxyphenyl]- । । I । , I r . . TTr । , . j . . 185 36.00 36.20 36.40 36.60 m/z 112.1.0 29.18% 5000 115 142z 63 89 I . .. ......... ........... miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 36.00 36.20 36.40 36.60

1440.D GCMS0308.M Mon Mar 25 08:22:47 2002 Page 3

NYC-WTC_000038630

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NYC-WTC_000038630Source: NYC Law Department, mirrored locally

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