GCMS analysis results for sample AE01440, Feb 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\1440.D Vial: 12 Acq On : 22 Feb 2002 12:56 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Octadecanoic acid Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.88 44.82 ug/1 3218550 Chrysene-dl2 33.80

Hit# of 5 Tentative ID MW Mol Form' CAS# Qual

1 Octadecanoic acid 284 C18H3602 000057-11-4 99 2 Heptadecanoic acid 270 C17H3402 000506-12-7 90 3 Tetradecanoic acid 228 C14H2802 000544-63-8 87 4 Hexadecanoic acid 256 C16H3202 000057-10-3 81 Abundance Scan 2706 (29.881 min): 1440.D (-) | m/ z 73.00..100.00% 60 73 43

5000 129 85 97 185 284 115 241 1 1 1 1 r 1 1 I ■ 1 ■ 1 i ' ■

m/z- —l—ulu—lLll—l— l 40 60 80 100 143 157 171 199 213 227 | 255267 T T ' 1 T TTT r TIHPm I ,, 'i । .... । t | m/ Z 120 140 160 180 200 220 240 260 280 29.60 29.80 30.00 30.20 43.05 96.68% Abundance #72366: Octadecanoic acid 43 57 73

5000 129 29.60 29.80 30.00 30.20 l 85 97 185 241 284 m/z 59.95 79.94% i : ILL 172 I 199 227 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 73 60 29.60 29.80 30.00 30.20 5000 m/ z 41.05 71.99% 129 85 97 . 227 115 171 185 270 ‘ 111111/111/1/1 ..... . . | I I > I | I I ! I | I 1 . . i ■ ■ > . I ■ ■ ■ ■ i > i 1 । I i । m/z-> 40 60..... 80..... 100... 120 140 160 ... 180.... 200 220 240 260 280 Abundance #29646: tetradecanoic acid 60 73 29.60 29.80 30.00 30.20 m/z 57.00 70.61% 5000 129 85 185 - Il 97 - 115 143 171 | --PPPI 228 ' i ' ■ ' 1 i 1 ' 1 1 i ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 29.60 29.80 30.00 30.20

1440.D GCMS0308.M Mon Mar 25 08:22:42 2002 Page 2

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