GCMS analysis results for sample AE01440, Feb 2002

NYC 9/11 Public Portal Document 2 ‘L

Data File : C:\HPCHEM\l\DATA\FEB2102\1440.D Vial: 12 Acq On : 22 Feb 2002 12:56 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hexadecanoic acid Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

27.49 16.31 ug/1 1555970 Phenanthrene-dl0 25.73

Hit# of 5 Tentative ID MW Mol Form' CAS# Qual

1 Hexadecanoic acid 256 C16H3202 000057-10-399 2 Pentadecanoic acid 242 C15H30O2 001002-84-2 80 3 Tetradecanoic acid 228 C14H28O2 000544-63-8 74 4 Dodecanamide, N,N-bis(2-hydroxyethy 287 C16H33NO3 000120-40-1 68 Abundance Scan 2446 (27.494 min): 1440.D (-) ! m/z 73.00 100.00% 43 73 60

5000 129 85 07 256 1 Y 115 143 157 171 185 213 27.20 27.40 27.60 27.80 — Jill, ula—ll 4—4—44+ - 199 | 227 239 ' i ‘ ‘ 1 ‘ i 1 T1.1 m/ z 43.05 82.57% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #71609: Hexadecanoic acid 43 60 73

> < | ■ i ■ ■ | 7 ■ • ■ | ■ 1 ' 1 | । ' 5000 129 ___ 27.20 27.40 27.60 27.80_____ | 85 97 i 157 171 185 213 256 m/z 59.95 79.46% I | j J 199 | 227 i ■ ' 1 ■ i 1 1 mz—20 _ 40 60 80 100 120 140 160 180 200 220 240 260 Abundance 43 60 73 TTT 1 1 27.20 27.40 27.60 27.80 5000 m/ Z 41.05 68.15% 242 27 129 85 97 143 157 171 — .4 185 199 214.............................. i‘1 ■'i■■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ * । * ■ > ■ । ■ - ■ • । . ■ ■ . । . । ■ ■ • ■ । ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #70841: Tetradecanoic acid 60 73 27.20 27.40 27.60 27.80 m/ z 57.00 58.77%

5000 - 129 27 85 185 228 1 , 97 i ■ ■ ■ 1 i ' 1 143 1712 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 27.20 27.40 27.60 27.80

1440 .D GCMS0308.M Mon Mar 25 08:22:38 2002 Page 1

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