GCMS calibration table for TCLP analysis, February 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1402\1045.D Vial: 8 Acq On : 14 Feb 2002 4:52 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Octadecanoic acid Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.87 4.49 ug/1 494936 Chrysene-dl2 33.82

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecanoic acid 284 C18H36O2 000057-11-499. 2 Heptadecanoic acid 270 C17H3402 000506-12-7 87 3 Hexadecanoic acid 256 C16H3202 000057-10-3 83 4 Pentadecanoic acid 242 C15H30O2 001002-84-2 83 Abundance Scan 2704 (29.865 min): 1045 D(-) m/z 43.05 100.00%

1 43 60 73

5000 129 65 97 284 T

miz-? 44 40 (60 4L -4 80 100 115

120 143 157 171 185 241 | 199 213 227 । 255 । ।। । i' । । ।। । i''i । । 'i r । '■ r । .A-. । i1’. Ibu 140 160 180 200 220 240 260 —L m/z 41.05 280 29.60 29.80 30.00 30.20 86.38% Abundance #72366: Octadecanoic acid * 57 73 5000 129 29.60 29.80 30.00 30.20 65 97 185 241 284 m/z 73.00 85.66%

m/z- ' i' ■ ■ ' i'1 ■ ’ i ’ 40 60 80 — 100 ..2% 227 140 160 180 200 220 240 260 120 280 Abundance 73 60 / TT _ 29.60 29.80_30.00 30.20_ 5000 m/z 60.05 ' 81.49% 129 35 97 . 115 171 135 227 270 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71607: Hexadecanoic acid 43 60 73 __ 29.60 29.80 30.00 30.20 __ m/z 55.00 74.53% 5000 256 129 [ 85 97 213 157 171 | 227 209—0999—— TII m/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 29.60 29.80 30.00 30.20

1045.D GCMS0308.M Thu Mar 14 15:29:35 2002 Page 1

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