GCMS calibration table for TCLP analysis, February 2002

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Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

NYC-WTC_000052630–000052637

Folder label: “GCMS X 1/15/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1402\1045.D Vial: 8 Acq On : 14 Feb 2002 4:52 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.33 357.97 ug/1 27754000 Perylene-dl2 38.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3/76 2 [1,1'-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-738 3 2,4,6(1H,3H,5H)-Pyrimidinetrione, 5 240 C12H20N2O3 051209-93-9 25 4 Pyridine, 4-[4-methoxyphenyl] - 185 C12H11NO 000000-00-0 17 Abundance Scan 3408 (36.328 min): 1045.D (-) m/z185.10100.00% 145 Ml 5000 57 । 112

m/z-> 24.124.442266, 203 223 242 268 297315 340 339 397 426 ■" I" " r' "i"'11'1' ■ ।।। 40 60 80 100120140160180200 220240260280 300 320 340 360380400420 ।i" " i" "I 36.00 36.20 36.40 36.60 m/z ’ 57.00 46.38% Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

57 ..... / t...... 5000 112 36.00 36.20 36.40 36.60 83 m/z 70.10 34.46% 143 166 । 203 298316 TTunna"uumnumnnnnun—n"nn"nnnnnmBBm—mB—B—“—05 m/z-> 40 60 80 100120140160180 200 220 240 260280 300 320 340 360 380400420 Abundance 185 — 36.00 36.20 36.40 36.60 5000 m/z 71.10 32.93% 156 128 r'" r i" " r •" i T‘001001110010001130103731010 ‘7110317101301113007181113777‘7771 m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400420 Abundance #31909: 2.4.6(1H,3H,5Hj-Pyrimidinetrione, 5.5-diethyl-1-(1- y ' ' I ' ' ' ' I 1 TI 185 36.00 36.20 36.40 36.60 m/z 112.10 28.67% 5000 211 70 I I mm96 114 155 240 r'" r " ’ i In"i11 ■ i""i" "r"'r "■ r ■ "i""r'"I"■'i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 36.00 36.20 36.40 36.60

1045.D GCMS0308.M Thu Mar 14 15:29:40 2002 Page 2

NYC-WTC_000052636

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GCMS calibration table for TCLP analysis, February 2002 · Box DEP Box 28

NYC-WTC_000052600

Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

Same agency, volume and box · similarity 0.995