GCMS blank analysis results for VOCs, March 2002

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Data File : C:\HPCHEM\1\DATA\MAR2202\LBB.D Vial: 31 Acq On : 23 Mar 2002 11:41 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ****************************************** * * ************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.20 7.66 ug/1 777698 Perylene-d12 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-376 2 [1,1’-Biphenyl]-4-ol, 3-amino- 185 C12H11NO। 001134-36-7 38 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO1 000000-00-0 17 4 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO1 000000-00-0 17 Abundance Scan 3394 (36.201 min): LBB.D (-) m/z 185.10 10 0.00% 1$5

5000 57 70 112 43 83 98 i ■ ' ' 1 i '

m/z->_ 40 111 60 +H 80 125 143 166 - —P........ P : 203 255268281 297 315 100 120 140 160 180 200 220 240 260 280 300 320 35.80 36.00 36.20 36.40 36.60_ m/z 57.00 4 0.94% Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 57 8 71 112 35.80 36.00 36.20 36.40 36.60 m/z70.10 32.29% 84 98 i | 125 143 166 TTR—dt—1OgOTDTOTDTTTTPITPTTTI 203 298 316 | 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 | Abundance -- .ma ■ ' T 185 I 1 1 ' 1 1 1 1 ' 1 I ' ' ■ ■ 1 1 1 35.80 36.00 36.20 36.40 36.60 5000 m/z 71.10 30.74% 139 156 113 1' ।11'11 ■'1 ■ i ‘ '11111' i111111 1 1........ । । । । i i । i i r i | । | m/Z“>___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ' Abundance #19197: Pyridine, 4-[4-methoxyphenylj- 185 35.80 36.00 36.20 36.40 36.60 m/z 112.10 26.60% 5000- 142 115 170 63 89 155 । .... । i । । /1 —— - ■ ‘ i1 1 ■ ■ i 1 1 ' 1 i ' 1 1 1 i ' 1T ' I ‘ 11 1 I 1 1 1 1 I ‘ 11 1 I ' 1 1 1 I 1 11 1 I 1 1 ' ‘ I 1 1 1 1 I 1 1 ' 1 I 1 ! m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 i 35.80 36.00 36.20 36.40 36.60

LBB.D GCMS0308.M Tue Mar 26 10:51:05 2002 Page 2

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