GCMS analysis results for sample AE08487, May 2002

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Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.

NYC-WTC_000023292–000023303

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY0902\8487.D Vial: 12 Acq On : 10 May 2002 1:12 am Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Decanedioic acid, bis(2-ethylh Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 36.13 27.50 ug/1 1282460 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic cid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 68 2 Propanedioi acid, hexyl-, diethyl 244 C13H2404 005398-10-7 27 3 [1,1’-Biphenyl]-4-ol, 3-amino- 185 C12H11NO1 001134-36-7 22 4 Octane, 2,5-dimethyl- 142 C10H22 015869-89-3 22 Abundance Scan 3392 (36.125 min): 8487.D (-) m/z 185.15 100.00% 185 57 5000 70 43 112 83 98 125 143 166 203 35.80 36.00 36.20 36.40 255268 297 315 oM 1" TTT 1r Arl r 110011; .t I. —1—-———n—2*000—Ou——adtu m/z 57. 10 64.88% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid, bis(2-ethyihexyl) ester 185

5000 57 71 112 35.80 36.00 36.20 36.40 m/z 70.15 44.37%

mfe-> 40 L 60 80 98 125 143 166 203 298 316 ‘I—T TTPTIITm TTTTTOguwwmTTTTI 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70 35.80 36.00 36.20 36.40 5000 m/z 71.10 43.57% 83 112

42 98 — ] p'1 ‘ ' I rl 1 1 1 1 ' L 199 217 1****11001101011011100000———- mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #19199: [1,1 ’-Biphenyl]-4-ol, 3-amino- । । । । 1 । IPITT । । । i । 185 35.80 36.00 36.20 36.40 m/ Z 43.05 36.32% 5000

139 156 ............... ..... 1 m >1 j ■ > ■ ■ i ■ ■ ■ > । । ■ 111 ■ * 111 ' i '| । । । 1 ■ | ' ' ' ' I ■ 1 ' ' I ' ‘ ' ' I ' ' ' ' ! ■ ' > ■ I ■ ' ‘ ' I ‘ 1 ' I ' 1 ■ ■ i ■ 1 ■ 1 i 1 1 ' ' i 1 1 1 1 i m/z—-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.80 36.00 36.20 36.40

8487.D GCMS0510.M Fri May 10 13:58:10 2002 Page 4

NYC-WTC_000023302

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NYC-WTC_000023372

Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.

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