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GCMS analysis results for sample AE08487, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.

NYC-WTC_000023292–000023303

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023301
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY0902\8487.D Vial: 12 Acq On : 10 May 2002 1:12 am Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 25.72 0.44 ug/1 40438 Phenanthrene-dl0 25.58

Hit# of 5 /Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 2 Phenanthrene-diO 3 Antipyrine 4 - (4-Tolyl) -3-methyl-pyrazol-5-one 188 188 188 188 C14D10 C14D10 C11H12N2O C11H12N2O 001719-06-8 001517-22-2 000060-80-0 38 035496-19-6 38 G Abundance Z Scan 2256 (25,716 min): 8487.D (-) m/z 188.15 100.00%| 188

5000

94 *........ .. 80 25.40 25.60 25.80 26.00 42 66 160 — -T - IJL. I"' m/z 94.10 19.10%| m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d1 0- 11)8

-- 5000 25,40 25.60 25.80 26.00 m/z 189.15 14.22% 80 94 160 • ■ | " I। . | . ■ , . I| , . , . | 11 I I I ' | ' I ! I m I' I I | I I I ! | ! I I I | > ‘I’’ miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 __ |T“. | ! I I I _____ | I 1 | I I

25.40 25.60 25.80 26.00 5000 m/ Z 80.10 13.65%|

80 94 160 ■...................... 66 miz-> 30 40 50 60 70 80 H 111111" ।"1 ■ ।" 111 >1 90 100 110 120 130 140 150 160 170 180 190 ...... W,.... Abundance . #69176: Antipyrine 188 25.40 25,60 25.80 26.00 m/z 184.15 12.41%| 96 5000 77 56 105 . ........................... 111' 1.116 129 159 173 1 ('1111' ■1 ■ 1I " " i1 " ' i " " i " " i ■ " ' i " " i'1 1U 1111 n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

8487.D GCMS0510.M Fri May 10 13:58:09 2002 Page 3

NYC-WTC_000023301

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NYC-WTC_000023301Source: NYC Law Department, mirrored locally

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