GCMS Sample AE03388 Report, March 12 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2102\3388.D Vial: 50 Acq On : 23 Feb 2002 5:22 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.87 0.23 ug/1 19844 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 64 2 Phenanthrene/diO ' 188 C14D10 001517-22-2 50 3 1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 40 4 Benzene, 1-bromo-4-methoxy- 186 C7H7BrO 000104-92-7 23 Abundance / Scan 2269 (25,874 min): 3388.D (-) m/z 188.10 “ 100.00% 188

5000 —

44 26 84 4 160 — 25.60 25.80 26.00 26.20 ------- 111'1 ■ ■ i ■ ■ I’T m/z 189.05 26.75% m/z~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-di 0- 188

5000 / - yi.. 25.60 25.80 26.00 26.20 80 94 m/ z 184.10 16.53% 66 160

m/z-> 40 50 60 70 80 90 100 110 120 130 1401‘‘‘‘1501‘1/11160‘‘441* 1' i' ■ ■ ■ i ■'1 ■ i ■ ■ ■ ■ i'1' ■ i ‘4*1//‘‘I+S 170 180 190 Abundance 188 ............... ...............................

25.60 25.80 26.00 26.20 5000 m/ z 93.85 15.26%

66 80 94 160 TTTTPTTIWTTTWTTWTmT)WTmTPT]m?WPWTPTTTTTIT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69174: 1,4-Naphthalenedione, 2-hydroxy-3-methyl- 188 25.60 25.80 26.00 26.20 m/ z 65.95 14.95% 5000

105 131 160 50 77 m/z-> ....... ...... |........ I'm-" '........ 40 50 60 70 ................................. .. .............. i' " 'i■1''i''1'i'''' i11'' ।' ■'' ।'' ■' | ■1'111111111 80 90 100 110 120 130 140 150 160 170 180 190 L A 25.60 25.80 26.00 26.20 IT

3388.D GCMS0208.M Fri Mar 08 09:45:18 2002 Page 2

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