NYC-WTC_000006328
Initial GCMS analysis report for sample AE03435 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS surrogate recovery data, Mar 12 2002
Machine-extracted title · confidence 90%Quality control page documenting surrogate compound recovery rates for a gas chromatography mass spectrometry run.
NYC-WTC_000006272–000006281Folder label: “GCMS X 2/14/02 A 2/23/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C : \HPCHEM\ 1 \DATA\ FEB2 1023385.D Vial: 47 Acq On : 23 Feb 2002 2:25 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
25.87 0.21 ug/1 20115 Phenanthrene-dl0 25.73
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Anthracene -d1- / 188 C14D10 001719-06-8 83 2 Phenanthrene d10 188 C14D10 001517-22-2 64 3 Phosphonic cid, (3-methyl-3-penten 188 C8H13O3P 022152-34-7 59 4 Pentacyclo L 4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 33 Abundance / Scan 2269 (25.872 min): 3385.D (-) ] m/z 188.10 ' 100.00% 188
5000
158 25.60 25.80 26.00 26.20 66 r— ■11' " ' I' m/z 189.10 18.84% mlz- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190i I A Abundance #19957: Anthracene-dlO- 188
5000 25.60 25.80 26.00 26.20 i m/z 93.90 16.48% TIwmmmmm9mmm0]PITTNTTTT 66 80 94 160 dl m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188 ......... .........
25.60 25.80 26.00 26.20 5000 m/z 8 3.00 16.30%
RR 80 94 160 bo ’’I’’AIJ’’’SI*’A+}’I’I’IIIIAAA+L’’’AI’’’+I+’’’l’’+’I’++’1’’+/11+’’1’41A1’’A’1**’’I4I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ............. ....... Abundance #19736: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-. dimet 1$8 25.60 25.80 26.00 26.20 m/z 9 . 90 13.54%
5000 77 62 35 47 93 109 155 ‘ 11 , |. ।..T.... 1.... 1 | ■ । ■ ■' ‘ ।11111" ■11 1 11 1 1 1 ‘ 1 1 1 1 1 1 ( ' 1 ' 1 1 1 ' 1 ' 1 1 ' ' ' I 1 ' ‘ ' I ' ' ' 1 I ' ’’’ | i । । » | ... b | i i Tut m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20
3385.D GCMS0208.M Fri Mar 08 09:42:56 2002 Page 3
NYC-WTC_000006280
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NYC-WTC_000006280Source: NYC Law Department, mirrored locally
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