GCMS analysis results for sample AE09446, May 2002

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Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.

NYC-WTC_000023372–000023382

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY0902\9446.D Vial: 13 Acq On : 10 May 2002 2:11 am Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.71 0.48 ug/1 40850 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracepe-dlO- A 4 188 C14D10 001719-06-8 83 2 Phenanthrene-diO X / 188 C14D10 001517-22-2 80 3 4H-Pyrido [1,2-a] pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 4 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 38 Abundance 7 Scan 2256 (25,713 min): 9446.D (-) m/z 188.15 100.00% 188

5000 .......... )............................ 94 1 ' I 1 1 r 1 i ■ ■ 1 1 i ■ 1 ■ ' i 1 1 ■ ■ i 80 66 158 25.40 25,60 25.80 26.00 44 52 —TTT ' l ■ ■ IH -IH— I ‘' I'' ■' 111 1 ' I 111 IH I " 1 ‘ I' 11 11" L m/ z 94.10 19.44% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 118

- 5000 25.40 25.60 25.80 26.00 m/z 189.15 15.52% 80 94 160 66 । —mTTTT । ■ ••■।■■• • । ■ * 1111■■।■■ > ■ । II’r m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

25.40 25,60 25.80 26.00 5000 m/z 80.10 14.43%

80 94 160 66 ■ i • ■ • ■। H ............ III,. 111 ■ ■ ■11 I1 .ma ■ i ■ ■ I ■ i1 miz- > 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19873:4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- ........ /I............................. 145 1(18 25.40 25.60 25.80 26.00 173 m/z 184.15 11.52%

5000 92

65 159 119 132....... ।11" 11 TTITTTTTTTTTTTTTTTETTTT 11111 " 11'1 '11''11 " 11111 " 1111 - | n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9446.D GCMS0510.M Fri May 10 13:58:29 2002 Page 3

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