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GCMS analysis results, sample AE09394, May 8, 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09394 with unknown compounds and surrogate data from May 8, 2002.

NYC-WTC_000043097–000043111

Folder label: “GCMS X 4/18/02 A 5/1/02

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Scanned page image, NYC-WTC_000043110
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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0102\9394.D Vial: 12 Acq On 1 May 2002 6:12 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

25.73 0.44 ug/1 36927 Phenanthrene-dl0 25.59

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Anthracene 7d10- 2 Phenanthrene-diO 5 188 C14D10 188 C14D10 001719-06-8 001517-22-2 3 4H-Pyridoll, 2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 4 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 Abundance Scan 2257 (25.725 min): 9394. D (-) m/z 188.15 100.00% 188

5000 .......... / ee 80 94 • • i r ■ ■ • । । 1 i ' ‘ ' 1 i ' ' 1 ' I 158 25.40 25.60 25.80 26.00 54 43 i - 66 .1 I I I I | I1! Ii t | I I I I | I ■ > I | r I I I 11 11 11 " 11 11 1111 i III।।| !!I|I —ll, ,., m/ z 94.10 17.90% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

.......... / 5000 ‘ 'I 1 1 1 1 I ' I ' ' 1 ■ i 1 ' 1 1 I 25.40 25.60 25.80 26.00 m/ Z 184.15 14.59%

11'1'' r 66 11'1' 1 80 94 I । > < < < | I । I I | I > ! > | 160 I 11 ' I | ! ! I > | ■ > ! ! | ! ! I ! | I > I I । I I I I | I I I r | I I I I

m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 / 1111--T1---1/1/=1/1/B/1—/T 25.40 25.60 25.80 26.00 5000 m/ z 80.10 14.15%

80 94 160 66 m/z-> 1 1 1 1 1 1 1 1 40 50 60 — 70 80 H (1 11 ■ I ■' 11 11 1 •' I • ■ ■' I •' I

90 100 110 120 130 140 150 160 170 180 190 ....... W... Abundance #19873: 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- .......... ..... ‘........................ ■ ' | 1 1 ■ ■ | । 1 | ' । 1 । | । । । 1 | 145 188 25.40 25.60 25.80 26.00 173 m/ Z 189.15 13.20%

5000 92

65

119 132 159 1 - n i r | Imapassspe | .......... / ...................... m/z-> 40 50 60 70 80 ■ । । n । । । । । । । । । । n । । । । ' | 1 ।

90 100 110 120 130 140 150 160 170 180 190 TIT 1 ]I I i i I i i। 7I I I I | I

25.40 25.60 25.80 26.00 । | ' I | I I

9394.D GCMS0501.M Thu May 02 12:03:11 2002 Page 5

NYC-WTC_000043110

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NYC-WTC_000043110Source: NYC Law Department, mirrored locally

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