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GCMS sample analysis summary, May 10, 2002

Machine-extracted title · confidence 90%

Summary of GC/MS analytical results for sample AE09674 processed on May 10, 2002, including surrogate recovery data.

NYC-WTC_000043590–000043599

Folder label: “GCMS X 3/26/02 No Analyses

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Scanned page image, NYC-WTC_000043598
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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0602\9674.D Vial: 14 Acq On 7 May 2002 5:02 am Operator: Sample GC/MS SCAN 4/24 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-diO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 25.72 0.43 ug/1 44538 Phenanthrene-dl0 25.57 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 Anthracene/dlO- 7 188 C14D10 001719-06-8 91 2 Phenanthrene-d10 188 C14D10 001517-22-2 3 Pentacyclo[8.4.0.0(3,7) .0 (4,14) .0(6 188 C14H20 000000-00-0 44H-Pyrido[1,2-a]pyrimidin-4-one,3-188C11H12 N2 0 Abundance 057773-19-0 28 Scan 2257 (25.719 min): 9674.D (-) m/z 188.15 100.00% 188

5000

80 94 ' ' I ' ' ' ' I 42 66 160 ।,: 25.40 25.60 25.80 26.00 TTIPTTT T I I | I I । I | I I I I - 111'r 111 r 11' i -H-TP m/ z 94.10 16.72% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 .. M...... 1 I I I I I I I I I I I I I I I I I I I I TT 25.40 25.60 25.80 26.00 m/ z 80.10 16.03% 66 80 34 160 ' 11 " 111 TTTTTITTTPTLTTTTTTTTTTTI /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 .... . ............ 25.40 25.60 25.80 26.00 5000 m/z 189.15 16.03%

80 94 160 66 m/z--> ■ I ‘ 40 ' 1 1 50 —H H 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ilaaasama . inns

Abundance #19959: Pentacyclo[8.4.0.0(3,7) 0(4,14).0(6,11 )]tetradecane ............ /................. 188 25.40 25.60 25.80 26.00 m/z 184.15 12.22%|

5000

79 92 117 106 131 145 159 173 > ! | I I I I | I I TT pi n ! | ) ! ! ! [ ! — TT । i r | i < I ! | ! | I I....I..... I..... TTu 1.. i । i i i i । ri i । । । । ri |T nT nn । i i .... /....... ■ ' | 1 ' ’ ' | 1 1 1 . । . i < . | b r i ! | m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9674.D GCMS0501.M Wed May 08 11:53:09 2002 Page 2

NYC-WTC_000043598

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