Initial GCMS analysis report for sample AE03389 conducted by analyst DLV on March 12, 2002.
NYC-WTC_000006302–000006310Folder label: “GCMS X 2/14/02 A 2/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\FEB2102\3389.D Vial: 51 Acq On : 23 Feb 2002 6:21 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Anthracene-dlO- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
25.88 0.24 ug/1 22222 Phenanthrene-dl0 25.74
Hit# of 5 Tentative / ID / MW MolForm CAS# Qual
1 Anthracene-diO/ 188 C14D10 001719-06-8 <86. 2 Phenanthrene-cal0 188 C14D10 001517-22-2 50 3 - (4-Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 Pentacyclo [8.4.0.0 (3,7) . 0 (4,14) . 0 (6 188 C14H20 000000-00-0 36 Abundance Scan 2269 (25.876 min): 3389. D (-) 1m/z188.10 100.00% l 188
5000
66 --- 80 94 160 .n.. 25.60 25.80 26.00 26.20
m/z-> 60 70 80 .00 -P 90 100 110 120 130 140 150 160 170 180 190... | m/z 94.00 22.91% Abundance #19957: Anthracene-d10- 188
5000 1 1 I 1 1 1 1 1 ' 1 i ■ 25.60 25.80 26.00 26.20 80 94 m/ Z 79.95 16.57% 66 160 r ■ i'1 ' ■ i ■ ' ■ ■ i ' -L m/Z- 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188 - 25.60 25.80 26.00 26.20 5000- m/z 189.10 14 .”88%
80 94 160 66 '■ I ' 1 1 1 I '• 1 1 I 1 ' 1 ' I 1 ■' 1 I ' 1 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I 1 ' 1 1 I 1 1 1 1 I ' 1 1 1 11 11 'I' m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one ........................... . 188 25.60 25.80 26.00 26.20 91 m/z 184.05 12.21% 105 5000 119 65 ... | - 78 146 | ' 1 i ■ ■ r ' i ' ‘ I ' 1 1 1 I ' । 1 1 I ' 1 1 1 I 1 1 1 1 I 1 1 ' 1 1 1 1।■। >>'।।11 1 1 । ' ' । । । । । III ............. m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20 j
3389.D GCMS0208.M Fri Mar 08 09:46:12 2002 Page 2
NYC-WTC_000006309
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NYC-WTC_000006272
Quality control page documenting surrogate compound recovery rates for a gas chromatography mass spectrometry run.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006292
Initial GCMS analysis report for sample AE03388 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005302
Laboratory report documenting GCMS analysis of sample AE02599 conducted on March 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005595
Laboratory report for DEP sample AE02789 showing unknown compounds and surrogate recovery data from March 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006337
Initial GCMS analysis report for sample AE03436 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006328
Initial GCMS analysis report for sample AE03435 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003753
GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038594
Gas chromatography-mass spectrometry analysis report for environmental sample AE04036 dated March 29, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038552
Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038837
Laboratory report documenting GCMS analysis of sample AE02578 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038314
Laboratory report documenting GCMS analysis of sample AE04025 conducted on March 15, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038532
Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000006246
Department of Environmental Protection GCMS sample tracking record for the World Trade Center site dated February 2002.
Filed in the same folder
NYC-WTC_000006247
Header page for a GCMS laboratory report series dated February 14 to 23, 2002.
Filed in the same folder
NYC-WTC_000006249
Laboratory report listing quantitative results for volatile organic compounds including nitrosamines and chlorinated solvents.
Filed in the same folder
Laboratory results for volatile organic compounds including nitrosamines and chlorobenzenes from sample AE03385.
Filed in the same folder
NYC-WTC_000006258
Calibration table and response data for polycyclic aromatic hydrocarbons and volatile organic compounds used in GCMS analysis.
Filed in the same folder