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GCMS analysis results for sample AE01440, Mar 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated March 29, 2002.

NYC-WTC_000038613–000038622

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000038621
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NYC 9/11 Public Portal Document LJJL a L y OUaLti LOIpUuU KtpUL L

Data File : C:\HPCHEM\l\DATA\MAR2202\1440.D Vial: 43 Acq On : 24 Mar 2002 11:32 am Operator: Sample : re-extract Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-diO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.79 0.25 ug/1 46562 Phenanthrene-dl0 25.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 72 2 Phenanthrene-dl0 188 C14D10 001517-22-2 40 3 4H-Pyrido [1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 38 4 Pentacyclo [8.4.0.0 Scan(3,7) . 0 (4,14) 2260 (25.790 min): 1440.D. (-) 0 (6 188 C14H20 000000-00-0 36 Abundance 188 m/z 188.10 100.00%

5000 - ........... -................... — 25.40 25.60 25.80 26.00 26.20 42 TTTITmTTTTTT 1‘I 66 80 24 160 m/ z 18 9.05 16.82% miz-2 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-dlO- 188

............ —................. — 5000 25.40 25.60 25.80 26.00 26.20 94 m/z 94.00 14.01% — 00 80। 160 1 111 > ■1111 1'111 3 111111111 — I ''' I'''' I'1' ‘ I'''1 I '1 1' I''1' I' ' miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

25.40 25.60 25.80 26.00 26.20 5000 m/z 80.05 13.87%

_ 80 94 100 66 97 ' I ' 1 ' 1 1 1 TIWTTIWTTTT r ■ ■ ■ ।111' i1 ■11111'11' ■ ’ ■ i' ■111'11111 ■111111111111111 m/z-> 40 50 60. 70 . 80 90_ 100 110 120 130 140 150 160 170 180 190 Abundance #19873: 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- 145 138 25.40 25.60 25.80 26.00 26.20 173 m/z 65-95 9.50% 5000 92

65 119 132 159 m/z-> H... PP 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 ' 1 I 1 1 1 1 I 1 1 1 rn 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 '1111111 11'11'1111111111T TTT -----.........— 25.40 25.60 25.80 26.00 26.20

1440.D GCMS0308.M Tue Mar 26 10:40:12 2002 Page 2

NYC-WTC_000038621

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NYC-WTC_000038621Source: NYC Law Department, mirrored locally

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