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GCMS analysis results for sample AE02789, March 11, 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02789 showing unknown compounds and surrogate recovery data from March 11, 2002.

NYC-WTC_000005595–000005603

Folder label: “GCMS X 2/6/02 A 3/1/02

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NYC 9/11 Public Portal Document IL D IP—

Data File C:\HPCHEM\1\DATA\MAR0102\2789.D Vial: 23 Acq On 2 Mar 2002 5:58 am Operator: Sample gc/ms scan 2/6 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Anthracene-dlO- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.25 ug/1 30300 Phenanthrene-dl0 25.71

Hit# of 5 'entative ID MW MolForm CAS# Qual 1 Anthracene -d1o- X$ 188 C14D10 001719-06-8 80 2 Phenanthrene-diO X 188 C14D10 001517-22-2 50 3 1,4-Naphth enedione, 2-hydroxy-3-m 188 CHH803 000483-55-6 50 4 3H-Pyrazol Scan2,4 -one, (25.852 min): 2789.D 4(-)-d 188 C11H12N2O 2267-dihydro-4, 017694-06-3 42 Abundance . ! m/z 188.10 100.00% ite /

5000 ----------- 94 159 66 78 25.60 25.80 26.00 26.20 TTP - ■ । ■ ■ ■ ■ j ■ T’’ m/ z 189.05 20.89% m/z->.. 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d'O- 188

................ .......... ................... 5000 25.60 25.80 26.00 26.20

.0680*.. .... J60.. . m/z 94.00 16.26%

m;z-> 4C 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

25.60 25.80 26.00 26.20 5000 m/z 159.05 14.39%

80 94 160 66 m/z-> 40 50 60 70 ' 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69174: 1,4-Naphthalenedione, 2-hydroxy-3-methyl- 188 25.60 25.80 26.00 26.20 m/z 160.05 12.03% 5000

77 105 131 16C 50 m/z-> 40 50 ,..... pl.... 60 70 80 .... ......... !|.... n.I. |. 11 * M 1111111 ■ ■'11111111111111 1’’ 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2789.D GCMS0208.M Tue Mar 05 10:54:20 2002 Page 1

NYC-WTC_000005602

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NYC-WTC_000005602Source: NYC Law Department, mirrored locally

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