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GCMS analysis results for sample AE02783, Mar 11, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02783.

NYC-WTC_000005525–000005534

Folder label: “GCMS X 2/6/02 A 3/1/02

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Scanned page image, NYC-WTC_000005533
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LLDLCLX DtaLCii topOuiU RCDOL L

Data File C:\HPCHEM\l\DATA\MAR0102\2783.D Vial: 17 Acq On 2 Mar 2002 12:06 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.27 ug/1 35636 Phenanthrene-dl0 25.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 83 2 Phenanthrene-d10 188 C14D10 001517-22-2 72 3 1,4-Naphtha! enedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 50 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 2267 (25.851 min): 2783.D (-) m/z 188.10.... 100.00% 183

5000 ....................................................

m/z-> 40 1.44."/ 52

50 60 66

70 80

80 94 TPPTTITTTTTTTTLTTTLTTTT 160 । m 90 100110120 130140 150 160 170 180190 25.60 25.80 26.00 26.20 m/z 184.05 17.96% Abundance #19957: Anthracene-d 10- 188

............ ......... 5000 25.60 25.80 26.00 26.20 80 94 m/z . 00 17.74% 160 66 011 TT-TT rn/z-> 40 50 60 70 80 44++ ' r " ' i1" ■ i " " i " 1111111111'111'1111" ''111 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

25.60 25.80 26.00 26.20 5000 m/z 189.10 17.74%

80 04 160 66 •*

m/z—> _ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ................... ................................. Abundance #69174: 1,4-Naphthalenedione, 2-hydroxy-3-methyl- 188 25.60 25.80 26.00 26.20 m/z 80.05 16.66% 5000

m/z-> 50 111"1111"111 40 50 60 70 80 105 ■ 131 ..... I|,,„..... „.160

90 100 110 120 130 140 150 160 170 180 190 T’r ................... ................................. 25.60 25.80 26.00 26.20

2783.D GCMS0208.M Tue Mar 05 10:47:22 2002 Page 2

NYC-WTC_000005533

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NYC-WTC_000005533Source: NYC Law Department, mirrored locally

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