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← Document results/DEP Box 25/GCMS X 4/29/02 A 5/3/02
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GCMS calibration results for TCLP method, April 25 2002

Machine-extracted title · confidence 100%

Calibration scan report for EPA Method 625 showing retention times and deviations for deuterated standards on April 25 2002.

NYC-WTC_000044621–000044627

Folder label: “GCMS X 4/29/02 A 5/3/02

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Data File : C:\HPCHEM\1\DATA\APR2 502\9330.D Vial: 7 Acq On : 25 Apr 2002 6:34 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 7:42 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.61 178 316 N.D. 35) Anthracene 25.60 178 539 N.D. 36) Di-n-butylphthalate 27.55 149 5854 N.D. 37) Fluoranthene 0.00 202 0 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 32.08 149 369 N.D. 4 2) Benzo(a)anthracene 33.65 228 3255 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 13105 0.40 ug/1 # 94 44) Chrysene 33.65 228 3999 N.D. 46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo(b)fluoranthene 36.70 252 280 N.D. 48) Benzo(k)fluoranthene 36.70 252 280 N.D. 49) Benzo(a)pyrene 37.87 252 3188 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9330.D GCMS0412.M Fri Apr 26 07:43:28 2002 Page 2

NYC-WTC_000044622

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NYC-WTC_000044622Source: NYC Law Department, mirrored locally

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