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GCMS analysis results for sample AE01440, Feb 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated February 22, 2002.

NYC-WTC_000038623–000038631

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document , LA1 L\DCL IC VLUWEU)

Data File : C:\HPCHEM\l\DATA\FEB2102\1440.D Vial: 12 4 Acq On : 22 Feb 2002 12 :56 am Operator : Sample : gc/ms scan 1/22 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 22 9:18 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 ' N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.80 178 193 N.D. 34) Anthracene 25.80 178 193 N.D. 35) Di-n-butylphthalate 27.70 149 15017 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.22 149 441 N.D. 41) Benzo(a)anthracene 33.80 228 1115 N.D. 42) Bis(2-ethylhexyl)phthalate 34.00 149 4820 N.D. 43) Chrysene 33.80 228 1115 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.09 252 1239 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1440.D GCMS0308.M Mon Mar 25 08:21:16 2002 Page 2

NYC-WTC_000038624

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NYC-WTC_000038624Source: NYC Law Department, mirrored locally

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