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GCMS calibration table for TCLP analysis, April 2002

Machine-extracted title · confidence 100%

Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.

NYC-WTC_000044700–000044707

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\APR2502\9335.D Vial: 12 Acq On : 25 Apr 2002 11:23 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 7:48 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.59 178 685 N.D. 35) Anthracene 25.59 178 685 N.D. 36) Di-n-butylphthalate 27.56 149 2391 N.D. 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.65 228 2730 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 20242 0.74 ug/1 95 44) Chrysene 33.72 228 801 N.D. 46) Di-n-Octylphthalate 35.60 149 589 N.D. 47) Benzo(b)fluoranthene 36.71 252 365 N.D. 48) Benzo(k)fluoranthene 36.71 252 365 N.D. 49) Benzo (a) pyrene 37.87 252 2561 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9335.D GCMS0412.M Fri Apr 26 08:23:27 2002 Page 2

NYC-WTC_000044701

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NYC-WTC_000044701Source: NYC Law Department, mirrored locally

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