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GCMS analysis results, sample AE09393, May 8, 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.

NYC-WTC_000043079–000043096

Folder label: “GCMS X 4/18/02 A 5/1/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0102\9393.D Vial: 11 Acq On 1 May 2002 5:16 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Phenanthrene-diO Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 25.72 0.44 ug/1 41379 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene/dl0 ( / 188 C14D10 001517-22-2 87 2 Anthracene-diO- / 188 C14D10 001719-06-8 72 3 2-Quinoline'carboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 38 44H-Pyrido[1,2-a]pyrimidin-4-one,3-188C11H12N20 7 057773-19-0 28 Abundance Scan 2257 (25.723 min): 9393.D (-) m/z 188.15 100.00% 188

5000

80 94 1 । | । i ii । r 1 ' 1 | * I I I । i । । । ।

mfe-> 39 52 66 '.......'11,11 + | I I f I | ! ! I I | ! ! Hi r I | > I ■ <

30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 I I | I . I I | ! I I I | I I I I । I I I I | I I —l— 25.40 25.60 25.80 26.00 m/ Z 80.05 19.99% Abundance #19958: Phenanthrene-d10 138

5000 1Til 25.40 25.60 25.80 26.00 m/z 94.10 18.43% 80 94 160 ■........................... 66 ——— m/z-> 30 40 50 60 70 A ppopp — > 11111 > 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 1 — m । । । i 1 ''' 1 i 25.40 25.60 25.80 26.00 5000 m/z 189.15 16.05%

66 80 34 160 .......... ... ..... | i i I i | i i । i | i TT n t I I I । I i । I I I I I | II I I | T' I I I | I r‘l "1"[ I I I I | rr I I | I I mr I I I | I I I I I I I I t I I I 1 I I I I I I mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime ................... ....................... ' ’ I 1 1 ' ' 1 1 1 ' 1 I 1 1 1 1 I 1 1 1 1 I 11)8 25.40 25.60 25.80 26.00 m/z 184.15 13.95%

5000

143 .64 89 116 130 ill T I I l n ! ! I | ' I I I I | ill 158 170 | 1 I ] I I — p i T i | I I i i |—।—।—i i—r i1'11 r 11' i' । । । । । । > । । i । i i i i । i । । ) । । । I । > 1 । । | I m । । । r I’r m/z--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9393.D GCMS0501.M Thu May 02 12:02:45 2002 Page 9

NYC-WTC_000043094

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NYC-WTC_000043094Source: NYC Law Department, mirrored locally

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