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GCMS analysis results for sample AE04036, Mar 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE04036 dated March 29, 2002.

NYC-WTC_000038594–000038603

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR2202\4036.D Vial: 44 Acq On : 24 Mar 2002 12:32 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.24 ug/1 40689 Phenanthrene-dl0 25.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene d10 188 C14D10 001517-22-2 72 2 Anthracene-d10- 188 C14D10 001719-06-8 64 3 1,4-Naphthdienedione, 5-hydroxy-2-m 188 C11H8O3 000481-42-5 37 4 Pentacyclo[8.4.0.0(3,7). 0(4,14) .0(6 188 C14H20 000000-00-0 33 ....... 1.... Scan 2261 (25.799 min): 4036.D (-) ...... Abundance |m/z188.10 100.00% 188

5000-

94 117 L..... i 1 11 * T ' 1 1 1 I 1 1 ,"1 1 1 1 66 80 156 . 25.40 25.60 25.80 26.00 26.20

m/z-? 40 11 111 ‘11 1 - - -H 1’’ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.00 21.24% Abundance #19958: Phenanthrene-d10 188

5000- .J 1 ■ I1 j -"11111118 25.40 25.60 25.80 26.00 26.20 m/z 189.10 18.77% 66 209 160 mTmTImmmmmmmnu N m/z-> 30 40 50 60 70 80 90 10 110 120 130 140 150 160 170 180 190 Abundance 188 ..... — 25.40 25.60 25.80 26.00 26.20 5000- m/z 184.05 14.18%

— 80 94 160 66

m/z->. 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19854:1,4-Naphthalenedione, 5-hydroxy-2-methyl- . 4 — —... 188 25.40 25.60 25.80 26.00 26.20 m/ z 80.00 10.54% 5000 - 63 92 131 120 51 77 160 173

— ' ' I 1''' I 103 1 I "‘III I > • ■■ l • < | T’ t J 1 | 25.40 25.60 25.80 26.00 26.20 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190

4036.D GCMS0308.M Tue Mar 26 10:49:34 2002 Page 2

NYC-WTC_000038602

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NYC-WTC_000038602Source: NYC Law Department, mirrored locally

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