GC/MS calibration table, sample AE08934, April 2002

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Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.

NYC-WTC_000043726–000043734

Folder label: “GCMS X 4/24/02 A 5/3/02”

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NYC 9/11 Public Portal Document —X -‘L

Data File : C:\HPCHEM\1\DATA\APR2302\8934.D Vial: 14 Acq On : 24 Apr 2002 3:05 am Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title 209 625/TCLP calibration table Library- C : \DATABASE\NBS75K . L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.72 0.22 ug/1 45808 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-^10. — 188 C14D10 001517-22-2 72 2 Anthracene-dl'0- / 4 188 C14D10 001719-06-8 53 3 Naphthalene/ 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 4 5 (4H) -Isoxazolone, 4,4 1 -bis [3-methy 376 C22H20N2O4 000000-00-0 33 Abundance 7 Scan 2252 (25.722 min): 8934.D (-) m/z 188.10 100.00% 188 N

5000 -------- 66 80 94 156 25.40 25.60 25.80 26.00 49 । ■ ■ ■ ■ i ■ ■ ■ ■ i mapamnsanns] 14 111 111111111111111 1111 I । । I l'| । " 1 I । 1b 'l " " I m/ z 189.10 13.93% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

1 I ] I I J, । T i — | I I I I | — I i 5000 25.40 25.60 25.80 26.00 m/Z 79.90 12.94% 80 94 160

m/z-> 40 i11 111' 50 60 P 66 70 80 H 90 100 110 120 130 140 150,160 170 180 190 11114 l Abundance #19957: Anthracene-d10- 188 ........................................... ' 1 I ' ' ' ' I ' 1 T ' 1 1 1 ' 1 1 1 ' 1 1 I 25.40 25.60 25.80 26.00 5000 m/z 184.10 11.96%

— 66 80 । 94 j TPTLTTTTTTTTTTTTTITPTTTTTTTPTTTTT 160 I... -- I I I ill I I ■ I I I I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- .......... )....................... 1 C I 1 I I I ! > > > I I I I . I I I I [■

173 188 25.40 25.60 25.80 26.00 m/ Z 94.00 10.79%

5000 115 145 102 51 63 75 94 130 158 । 11O1m]unu]uupummeTmghr TT T—umT—m l........ I " 1111 1 i1 ■ ■ ■ i m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25,40 25.60 25.80 26.00

8934 .D GCMS0412.M Wed Apr 24 08:38:55 2002 Page 3

NYC-WTC_000043733

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