GC/MS calibration table, sample AE08934, April 2002

NYC 9/11 Public Portal Document J ‘ L

Data File : C:\HPCHEM\l\DATA\APR2302\8934.D Vial: 14 Acq On : 24 Apr 2002 3:05 am Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.31 ug/1 59615 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual -I----------- 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6/8. 2 N-(Trifluoracetyl)-O, O 1 ,0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 38 3 Phenethylamine, N-methyl-.beta,,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 3 8 Abundance 73 7 Scan 1063 (14.807 min): 8934.D (-) m/z 73.00 100.00%

5000 267 355

1 14.40 14.60 14.80 15.00 15.20 45 108 154 193 237, 1. 323 — TP- m/z 3 55.05 46.55% TT— I I I I I I I I 1 I I I I

n/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 ........ / ......... 5000 I I I I I 1I■ I I I I I I I I I I I I I ‘ I

14.40 14.60 14.80 15.00 15.20 m/z 267.00 42.85% 207 323 1 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)epin 73 355 ....... 1 ' ' I ‘ ' I 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 15.91%

45 ii 140 184 281................. 480 ' 1 i 1 ti ■ r1 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls ........ /| , , , ..... . , 73 14.40 14,60 14.80 15.00 15.20 m/z 2 68.00 11.69%

5000 355

44 1 147 193 267 294 .................. / j i । i -'f | i i I । i r i r“ | ’ r ’i i i । i t I i ' । i i i i । i I I I | I I t i । i I 1 I | I I 1 ' ' ‘ I 1 1 1 ' I m/z-> 50 100 150 200 250 300 350 400 450 500 14.40 14.60 14.80 15.00 15.20

8934.D GCMS0412.M Wed Apr 24 08:38:54 2002 Page 2

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