GCMS calibration table, April 24, 2002

NYC 9/11 Public Portal Document ‘E

Data File : C:\HPCHEM\1\DATA\APR2302\8838.D Vial: 7 Acq On : 23 Apr 2002 8:17 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.42 ug/1 80959 Naphthalene-d8 15.84 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 cyclopentasiloxne, decamethyl- 000541-02-6/90/ 370 C10H3005Si5 2 Benzoic acid, , 5-bis (trimethylsilo 370 C16H30O4Si3 003618-20-0 43 3 N- (Trifluoroa tyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 43 4 N-(Trifluoroa^etyl)-0,0',0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 Abundance Scan 1063 (14.806 min): 8838.D (-) m/z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 i. , 103 154 191 223 . .l . । 323 . m/ z 2 66.90 1 1 । 43.71% m/z—>______ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / 5000 1 1 i 1 1 14.40 14.60 14.80 15.00 15.20 m/z 355.05 38.66% 207 323 Ut+ ■ ? ■ * ■ ■ । । ■ i ■ ■ ■ • । ■ ■ ■ ■ । । । । I ■

m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 15.67%

45

I I I I I k I I I I ,147 179 223 I I I I I I I I I I I I 267 297 I I I I I I I I I I I I । । । । r T’ i' | iir । d i i — i i

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi IB I 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 9.59% 355 5000

45 | 147 193 267 538 1 1 । 1 1 1 I | I I kil TT r 1 ""f" • I IT j Tl f i । i | | | |I | I" I' ' | " f I | | | J T 1 1 I ’ ' ' ' I ' ' ' 1 i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

8838.D GCMS0412.M Wed Apr 24 08:37:02 2002 Page 2

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